Original Contribution COENZYME Q 10 ENRICHMENT DECREASES OXIDATIVE DNA DAMAGE IN HUMAN LYMPHOCYTES M. TOMASETTI,* G. P. LITTARRU,* R. STOCKER, and R. ALLEVA* *Institute of Biochemistry, Faculty of Medicine, University of Ancona, via Ranieri, 60131 Ancona, Italy; Heart Research Institute, Camperdown, Sidney, New South Wales, Australia (Received 1 March 1999; Revised 26 April 1999; Accepted 28 May 1999) Abstract—Ubiquinol-10, the reduced form of coenzyme Q 10 , is a powerful antioxidant in plasma and lipoproteins. It has been suggested that endogenous ubiquinol-10 also exerts a protective role even towards DNA oxidation mediated by lipid peroxidation. Even though the antioxidant activity of coenzyme Q 10 is mainly ascribed to ubiquinol-10, a role for ubiquinone-10 (the oxidized form), has been suggested not only if appropriate reducing systems are present. To investigate whether the concentration of ubiquinol-10 or ubiquinone-10 affects the extent of DNA damage induced by H 2 O 2 , we supplemented in vitro human lymphocytes with both forms of coenzyme Q 10 and evaluated the DNA strand breaks by Comet assay. The exposure of lymphocytes to100 MH 2 O 2 resulted in rapid decrease of cellular ubiquinol-10 content both in ubiquinol-10-enriched and in control cells, whereas -tocopherol and -carotene concen- tration were unchanged. After 30 min from H 2 O 2 exposure, the amount of DNA strand breaks was lower and cells’ viability was significantly higher in ubiquinol-10-enriched cells compared with control cells. A similar trend was observed in ubiquinone-10-enriched lymphocytes when compared with control cells. Our experiments suggest that coenzyme Q 10 in vitro supplementation enhances DNA resistance towards H 2 O 2 -induced oxidation, but it doesn’t inhibit directly DNA strand break formation. © 1999 Elsevier Science Inc. Keywords—Ubiquinol-10, Ubiquinone-10, Coenzyme Q 10 Supplementation, DNA damage, Comet assay, Hydrogen peroxide, Lymphocytes, Liposomes, Free radicals INTRODUCTION Oxidative damage to DNA can result from free radical attack after exposure to ionizing radiation or to agents such as H 2 O 2 that can produce active oxygen species. The hydroxyl radical is thought to be responsible for most of the damage, such as strand breaks and the formation of oxidized bases. Endogenous damage to DNA, caused by oxygen free radicals liberated during normal respiration, may be significant in the etiology of cancer [1]. DNA damage can account for the genetic changes that occur at the different stages in the progres- sion from anaplastic growth to metastasis [2], and there- fore, dietary factors that reduce the impact of free radical attack are likely to protect against cancer. Antioxidants, largely of dietary origin, may limit DNA damage by scavenging free radicals and hence protect against mu- tagenesis and cancer [1]. Coenzyme Q 10 has long been known to be a compo- nent of the mitochondrial respiratory chain [3]. Recently, its reduced form (ubiquinol-10) has also been shown serve as a potent antioxidant, protecting phospholipids from peroxidation [4]. Recent investigations suggest that the endogenous content of coenzyme Q 10 might protect membrane proteins and DNA against oxidative damage mediated by lipid peroxidation [5– 6]. Although the an- tioxidant activity of coenzyme Q 10 in systems as lipopro- teins [7,8] or plasma [9], is mainly ascribed to ubiquinol- 10, an antioxidant role for ubiquinone-10 appears feasible even if appropriate reducing systems are not present. The aim of this study was to investigate the role of in vitro supplementation with both the reduced and oxi- dized forms of coenzyme Q 10 (i.e., ubiquinol-10 and ubiquinone-10, respectively) in the prevention of DNA oxidative damage in lymphocytes exposed to H 2 O 2 . Address correspondence to: Marco Tomasetti, Institute of Biochem- istry, School of Medicine, University of Ancona–via Ranieri-60131, Ancona, Italy. Tel./Fax: +390 735-592755; E-Mail: ralleva@jth.it. Free Radical Biology & Medicine, Vol. 27, Nos. 9/10, pp. 1027–1032, 1999 Copyright © 1999 Elsevier Science Inc. Printed in the USA. All rights reserved 0891-5849/99/$–see front matter PII S0891-5849(99)00132-X 1027