ORIENTAL JOURNAL OF CHEMISTRY
www.orientjchem.org
An International Open Access, Peer Reviewed Research Journal
ISSN: 0970-020 X
CODEN: OJCHEG
2022, Vol. 38, No.(2):
Pg. 388-398
This is an Open Access article licensed under a Creative Commons license: Attribution 4.0 International (CC- BY).
Published by Oriental Scientifc Publishing Company © 2018
A Study on the Effect of Lawsone as Complexing
Agent in the Electroless Zn-P Deposition
H. ASIA THAbASSOOM
1
*, F. FEMINA, J. FELICITA FLORENCE
2
,
R. KANMANI and J. AMALA INFANT JOICE
*
1,2
PG and Research Department of Chemistry, Holy Cross College (Autonomous),
affliated to Bharathidasan University, Tiruchirappalli-620002, India.
*Corresponding author E-mail: asia.shahbir@gmail.com
http://dx.doi.org/10.13005/ojc/380221
(Received: January 31, 2022; Accepted: April 6, 2022)
AbSTRACT
The effect of Lawsonia inermis Linn Leaf extract on electroless deposition of Zinc-P alloy
on mild steel is studied in alkaline solutions. The effect of experimental processing parameters on
the deposition rate is investigated during electroless plating. The bath compositions and operating
conditions are optimized. The results obtained show the inclusion rate of electroless Zn-P alloy coating
is found to be increased by increasing the volume of additives from 0.5 mL to 1.5 mL. Structured
UV-A signifcant spectroscopic absorption rate is taken to ensure the presence of Lawsone in the
binary complex in the alkaline bath. In the absence of a complexing agent, additive Lawsone develops
more features and levels of arrangement. It offers the idea of changing sodium citrate with Lawsone.
The effect of Lawsone as a complex agent on Zn-P electroless coating is tested by SEM, EDAX,
AFM, XRD and corrosion studies. The corrosion effciency of electroless Zn-P coating is assessed
by polarization and electrochemical impedance spectroscopy.
Keywords: Lawsonia inermis Linn leaf, SEM, EDAX, XRD, AFM, Micro hardness,
UV-Visible spectrum and polarization studies.
INTRODUCTION
Electroless plating of metals and process
technology have important role along with other
methods of plating. Electroless process is not
constrained by the shape, size or conductivity of
the supporting substance
1-3
. It is a highly effective
means of plating metals into nonconductors.
Hence electroless plating has elicited much interest
among scientifc community in recent years. Today,
sophisticated electroless plating systems are in
use in many varied electronic applications (PCB
industries, IC fabrication, EMI shielding etc)
4
.
Electroless plated zinc coatings are
considered as one of the many ways of corrosion
protection of steel. Zinc has many functions. It is
widely used in a variety of covering methods for the
protection of various metals, as well as in powder
and dust formulations, such as oxide, and for clinical
purposes
5
. Zinc is cut into dry batteries and hardens
the copper covering the U.S. penny. Zinc alloys are