S1
Cyclometalated iridium complexes for transfer hydrogenation
of carbonyl groups in water
Yawen Wei
a
, Dong Xue,*
a
Qian Lei,
a
Chao Wang
a
and Jianliang Xiao*
a,b
a
Key Laboratory of Applied Surface and Colloid Chemistry of Ministry of Education,
School of Chemistry & Chemical Engineering, Shaanxi Normal University, Xi’an,
710062, P. R. China.
E-mail: Xudong_welcome@snnu.edu.cn
b
Liverpool Centre for Materials & Catalysis, Department of Chemistry, University of
Liverpool, Oxford Street, Liverpool, L69 7ZD, UK
Fax: 44-151-7943588
E-mail: j.xiao@liv.ac.uk
Supporting Information
1. General information S2
2. General procedure for preparation of cyclometalated complexes S2
3. pH effect on transfer hydrogenation of acetophenone with
precatalyst 1 and 2 in water S2
4. General procedure for the reduction of ketones with the
precatalyst 3 S4
5. General procedure for the reduction of aldehydes with the
precatalyst 3 S4
6. Procedure for large scale transfer hydrogenation in water S5
7. Analytic data of catalysts and products S5-S13
8. References S14
9. Traces of
1
H NMR and
13
C NMR spectra S15-S45
Electronic Supplementary Material (ESI) for Green Chemistry
This journal is © The Royal Society of Chemistry 2013