https://doi.org/10.1177/0734242X20935174
Waste Management & Research
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© The Author(s) 2020
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DOI: 10.1177/0734242X20935174
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Introduction
In different societies, especially in developing countries, energy
consumption in various industrial and transport sectors is
increasing. The primary source for energy supply is fossil fuels
(Balmaceda, 2018; Marques et al., 2018). But the major prob-
lem with the planet’s atmosphere through burning these fuels is
damage to the ozone layer with emission of gases such as CO,
CO
2
and NOx. The devastating effects of these gases on envi-
ronmental pollution, ozone destruction and human health are
not hidden (Thangavelu et al., 2015; Wang et al., 2017). Even if
the problem of harmful gaseous emissions to the environment
can be controlled, fossil fuel sources will be exhausted in a few
decades (Barreto, 2018). Biofuels can be a good alternative to
these fuels and are environmentally friendly, renewable and
biodegradable. Biodiesel is the most commercial of them (Isa
and Ganda, 2018; Othman et al., 2017). Biodiesel is composed
of methyl ester of fatty acid (FAME) and can be produced in
several ways such as transesterification, pyrolysis, blending
and micro-emulsions (Gebremariam and Marchetti, 2017).
Transesterification or alcoholysis is more common; it is a reac-
tion between vegetable oil (or animal fat) and an alcohol,
mainly methanol or ethanol, in the presence of a catalyst
(Mumtaz et al., 2017). The main reaction product is biodiesel
along with glycerol as a by-product (Monteiro et al., 2018). In
addition to the significant advantage of biodiesel, it can be a
major energy source for diesel machines and, compared with
fossil fuels, burning it in engines produces less gas containing
hydrocarbons, polycyclic aromatic hydrocarbons and NOx into
the atmosphere (Ajala et al., 2015). Nevertheless, biodiesel can
face some economic difficulties. One of them is the high price
of feedstock which represents about 70–80% of the ultimate
cost (Ambat et al., 2018). To remove this as a challenge, using
waste edible-oil (waste frying oil), non-edible oil (algae oil,
soursop seed oil) (Dai et al., 2014; Su et al., 2018), insect fat
(Nguyen et al., 2018b) and waste animal fat (sheep, cow and
pig) can be helpful because they are cheap and available in the
restaurants. Waste frying oil is one example, which is discarded
after use. Using it reduces biodiesel production costs by 60–
90% (Fadhil et al., 2017; Rezania et al., 2019). The first group
includes soybean oil, palm oil, sunflower oil and sesame oil and
the second group includes oils like algal oil, jatropha, rape seed
and canola oil (Mardhiah et al., 2017; Verma and Sharma,
Low-cost biodiesel production
using waste oil and catalyst
Raheleh Talavari, Shokoufe Hosseini and GR Moradi
Abstract
With the production of renewable biofuels, concerns about the end of fossil fuels have been partially eliminated. On the other hand,
the utilization of low-cost and waste materials to provide the raw essential substances to manufacture these fuels is of paramount
importance. Biodiesel is one of these fuels and the required raw materials for the reaction are oil (triglycerides), alcohol and catalyst.
In this work, travertine stone powder (as waste in the manufacture of building materials) was used as a catalyst and waste frying oil
as a source of triglyceride for biodiesel production. Using thermogravimetric and X-ray diffraction analysis, optimum temperature
for catalyst calcination was selected at 900°C. Furthermore, X-ray fluorescence, Fourier transform infrared spectroscopy, Brunauer–
Emmett–Teller, transmission electron microscopy and scanning electron microscopy analyses were performed. Using the design
of experiments Response Surface Methodology, the optimum reaction conditions for biodiesel production yield of 97.74% were:
reaction temperature 59.52°C (~60°C), time 3.8 h (228 min), catalyst concentration 1.36 wt.% and the methanol to oil molar ratio of
11:6. After reusing four times, the catalyst efficiency was reduced a little, and the biodiesel yield was 89.84%, indicating high strength
and stability of the catalyst.
Keywords
Biodiesel, travertine, waste catalyst, waste cooking oil, transesterification
Received 9th March 2020, accepted 25th May 2020 by Associate Editor Mario Grosso.
Catalyst Research Center, Razi University, Iran
Corresponding author:
GR Moradi, Catalyst Research Center, Faculty of Chemical and
Petroleum Engineering, Razi University, Tagh Bostan, Kermanshah
6714414971, Iran.
Email: gmoradi@razi.ac.ir
935174WMR 0 0 10.1177/0734242X20935174Waste Management & ResearchTalavari et al.
research-article 2020
Original Article