Research Article Open Access
Volume 2 • Issue 1 • 1000121
J Environment Analytic Toxicol
ISSN:2161-0525 JEAT an open access journal
Open Access Research Article
Singh et al., J Environment Analytic Toxicol 2012, 2:1
DOI: 10.4172/2161-0525.1000121
*Corresponding author: Dharam Singh, Department of Environmental Sciences,
Institute of Bioscience and Biotechnology, C S J M University, Kanpur (UP),
India-208024, E-mail: ds_envi@rediffmail.com
Received November 13, 2011; Accepted January 03, 2012; Published January
05, 2012
Citation: Singh D, Katiyar S, Verma A (2012) Role of Copper Sulphate on Oxidative
and Metabolic Enzymes of Freshwater Fish; Channa Punctatus. J Environment
Analytic Toxicol 2:121. doi:10.4172/2161-0525.1000121
Copyright: © 2012 Singh D, et al. This is an open-access article distributed under
the terms of the Creative Commons Attribution License, which permits unrestricted
use, distribution, and reproduction in any medium, provided the original author and
source are credited.
Role of Copper Sulphate on Oxidative and Metabolic Enzymes of
Freshwater Fish; Channa Punctatus
Dharam Singh
1
*, Shashwat Katiyar
2
and Anju Verma
1
1
Department of Environmental Sciences, Institute of Bioscience & Biotechnology, C S J M University, Kanpur – 208024
2
Department of Biochemistry, Institute of Bioscience & Biotechnology, C S J M University, Kanpur – 208024
Keywords: Metal pollution; Fish; Organs; Enzymes; Tissue damage
Introduction
Present day heavy metal pollution has become global concern.
Te early detection of heavy metal ions, especially bioavalable metal
ion, in the environment is very important to safeguard to human
health. Copper is an essential trace metal in small quantity for
several fsh metabolic functions. Essentiality of copper arises from its
specifc incorporation into a variety of enzymes such as peroxidase,
xanthine oxidase, invertase, glucose oxidase and protease papain and
bromelain [1,2] which play important roles in physiological processes
(e.g. enzymes involved in cellular respiration, free radical defense,
neurotransmitter function, connective tissue biosyntheses and other
functions), as well as, proteins. Copper is used today a chemotherapeutic
agent in aquaculture however, the increased level of copper in aquatic
environments coming from sewage, industries (electroplating, mining
and metallurgy) and agricultural wastes [3,4]. Metals can either increase
or decrease hepatic enzyme activities and can lead to histo-pathological
hepatic changes, depending on the metal concentration, fsh species,
and length of exposure period [5]. Transaminase enzymes play vital
role in carbohydrate-protein metabolism in fsh tissues [6]. Changes in
enzymes activity and other biomarkers have been studied as possible
tools for aquatic toxicological research [7].
Increasing population, industrialization and agricultural
production has resulted in increasing the number of freshwater systems
which are being impaired by the contaminants present in wastewater
releases [8,9]. Micronutrient interact with toxic metals at several points
in body, absorption and excretion of toxic metals, transport of metals
in body, binding to target proteins, metabolism and sequestration of
toxic metals, and fnally in secondary mechanisms of toxicity such as
oxidative stress. Copper speciation is directly afected by water pH, and
the free cupric ion concentration is higher in water with low pH, while
a copper hydroxide complex prevails in water with high pH [10,11].
Te aim of present study was to evaluate efect on metabolic
indicators by sub-acute concentration of copper sulphate to
a freshwater fsh, Channa punctatus. Te efects on organ
were assessed by ALAT, ASAT, CAT and protein content.
Materials and Methods
Experimental groups
Te metabolic indicator efect of copper was studied by static
bioassay using tap water (University water supply) as dilution medium
was estimated by the method of APHA [12]. Te changes in physico-
chemical characteristics, such as temperature, pH, TDS (total dissolved
solids), DO (dissolved oxygen), hardness, alkalinity, chloride and iron
of experimental water were recorded throughout the experimental
period. Te small size freshwater fsh, Channa punctatus, weighing
15±2 g and measuring11±2 cm, were collected with the help of local
fsherman from water bodies located in the sub-region of Lucknow.
Te fsh was properly washed in tap water and treated with 0.02%
KMNO
4
and 0.004% formalin solution to remove external infection of
fungi and algae. Prior to the experimentation the normal uninfected
healthy fshes were selected for experiment. Te fsh were acclimatized
to laboratory conditions 15 days before taken for experimentation.
Te animals were fed fsh (TOKYO) made in Japan on each day in
the evening. Te LC
50
was estimated employing Trimmed Spearman
Karber Method [13] as 3.60 mg l
-1
. Te sub-lethal dose (0.36 mg l
-1
) was
related for exposure to fsh for 15, 30 and 45 days.
Design of sub-lethal toxicity study
Te fshes were divided into 4 equal groups consisting of 10 each
and each group was transferred separately to glass aquaria of 100 L
volume. While the Group I fshes were maintained as control without
any treatment, the Group II, III and IV fshes were exposed to sub-
Abstract
The effect of copper sulphate on liver, gills and kidney of fsh Channa punctatus was observed as metabolic
indicators. The fsh were exposed to sub-lethal (0.36 mg l
-1
) concentrations for 15, 30 and 45 days. The observations
revealed that in the presence of copper sulphate the metabolic enzymes aspirate amino transferases (ASAT) and
alanine amino transferases (ALAT) can enhance their activity, while catalase activity signifcantly reduced in response
to elevated level of superoxide production in exposed fsh as compared to healthy subjects. The major effect of
copper sulphate toxicity on exposed fsh shows as reduced amount of protein content as compared to unexposed fsh.
However, ASAT level have a signifcant negative correlation between catalase activity (r = 0.833, t = 6.3872, p 0.05)
and protein content (r = 0.8916, t = 8.3540, p 0.05) in the exposed organs. These fndings suggest that the signifcant
increase of transaminase activity while reduced amount of catalase and protein content might be the consequences of
tissue damage in Channa Punctatus.
Journal of Environmental &
Analytical Toxicology
J
o
u
r
n
a
l
o
f
E
n
v
i
r
o
n
m
e
n
t
a
l
&
A
n
a
l
y
t
i
c
a
l
T
o
x
i
c
o
l
o
g
y
ISSN: 2161-0525