Paper RADIOACTIVE ROCK PHOSPHATE: THE FEED STOCK OF PHOSPHATE FERTILIZERS USED IN PAKISTAN M. Tufail,* Nasim Akhtar, and M. Waqas Abstract—The existence of natural radioactivity in phosphate fertilizers originates from the rock phosphate that is used as a feed stock for the manufacturing of various types of phosphate fertilizers. Gamma ray activity mass concentrations have been determined in phosphate rock and fertilizer samples collected from different fertilizer manufacturing factories and suppliers in Pakistan. The technique of gamma ray spectrometry was applied using a HPGe (high purity germanium) gamma ray detector coupled with a personal computer (PC) based mul- tichannel analyzer (MCA). The specific activity values of 40 K, 226 Ra, and 232 Th were widely distributed in the rock and fertilizer samples. Activity mass concentrations of 238 U( 226 Ra) in the rock phosphate from Jordan and Pakistan were 428 11 and 799 10 Bq kg 1 , respectively, and that in the triple-superphosphate fertilizer was 701 21 Bq kg 1 , which was greater than the average values of 238 U( 226 Ra) for other types of fertilizers under study. The concentrations of 40 K and 232 Th were of the order of background level on the Earth’s crust. Chemical analysis for concentration of different constit- uents in rock phosphate was also carried out. The higher the concentrations of P 2 O 5 and K 2 O were, the higher the specific activities of 226 Ra and 40 K were, respectively, in the rocks under study. The amount of radioactivity in the rock phosphate is a source of continuous exposure to radiation, which varies widely depending upon the origin and grade of rock; therefore, radiation dose rate has been estimated. The values of dose rate and other derived quantities were many folds larger than the limits specified for those quantities. Health Phys. 90(4):361–370; 2006 Key words: dose assessment; 40 K; 226 Ra; 232 Th INTRODUCTION ROCK PHOSPHATE (P 2 O 5 ) is a terrestrial source of NORM (naturally occurring radioactive material) whose concen- tration varies from one place to another on the Earth; therefore, efforts are being undertaken to determine the amount of radioactivity associated with P 2 O 5 throughout the world. A substantial amount of radioactivity is transferred to fertilizers manufactured of phosphate rock (Bhatti and Malik 1994). The radionuclides that exist in the fertilizers are 238 U, 235 U, 232 Th decay series, and 40 K. Activity mass concentrations of natural radionuclides in phosphate fertilizers have been reviewed in the UN- SCEAR (1982) report where it has been concluded that for a given radionuclide and the type of fertilizers, the activity mass concentrations vary remarkably from one country to another, depending on the origin of the components. Sedimentary rock deposits supply about 80 – 85% of the P 2 O 5 as a raw material for manufacturing phosphate fertilizers throughout the world. Igneous type rock phos- phate deposits supply the remaining 15–20% of P 2 O 5 to the fertilizer industry (Awadalla and Habshi 1985). Rock phosphate of sedimentary origin contains on average 0.015% U 3 O 8 (Hussein 1994). The world consumption of phosphate fertilizers is about 60 million tons of P 2 O 5 (UNSCEAR 1993). The application rate of fertilizers depends on, among other things, the type of soil and the type of crop. The average consumption of phosphate fertilizers per unit area of agricultural land varied from 3.6 kg P 2 O 5 per hectare in the developing countries to 10.9 kg P 2 O 5 in the developed countries, the world average being 6.7 kg per hectare (UNSCEAR 1993). Human beings are exposed from many pathways to radioactivity present in phosphate rock. Phosphate rock, which is processed to make phosphate products, contains relativity high concentrations of naturally occurring ra- dionuclides, and the radioactivity in phosphate rock propagates in various amounts to all the phosphate products and byproducts (Hartley and Freeman 1986). It has been reported by Habshi (1985) that about 80% of rock phosphate is being used as a raw material for the manufacturing of phosphate fertilizers including phospho-gypsum, whereas the remaining 20% is being utilized for production of phosphorus compounds such as detergents, metal surface treatment reagents, chemicals for food industry, etc. The external exposure is to gamma * Pakistan Institute of Engineering and Applied Sciences, P.O. Nilore, Islamabad, Pakistan; Health Physics Division, NIAB, Jhang Road, Faisalabad, Pakistan; Department of Earth Sciences, Quad-i- Azam University, Islamabad, Pakistan. For correspondence or reprints contact: M. Tufail, Pakistan Institute of Engineering and Applied Sciences, P.O. Nilore, Islamabad, Pakistan, or email at dr_mtufail@yahoo.com. (Manuscript received 31 March 2005; revised manuscript re- ceived 28 July 2005, accepted 19 November 2005) 0017-9078/06/0 Copyright © 2006 Health Physics Society 361