ISSN 1062-8738, Bulletin of the Russian Academy of Sciences. Physics, 2014, Vol. 78, No. 4, pp. 330–332. © Allerton Press, Inc., 2014.
Original Russian Text © R.B. Abylkalykova, A.V. Dzhes, L.I. Kveglis, F.M. Noskov, M.N. Volochaev, A.G. Cherkov, 2014, published in Izvestiya Rossiiskoi Akademii Nauk. Seriya
Fizicheskaya, 2014, Vol. 78, No. 4, pp. 504–507.
330
INTRODUCTION
Fe
86
Mn
13
C alloy is known as Hadfield steel and is
widely used in industry and machine building due to
its low cost.
This alloy is known as an antiferromagnetic invar
[1]. Due to the spontaneously appearing regular com-
position of structures of antiferromagnetic austenite
and ferromagnetic deformation martensite, it can have
unique mechanical, electrical, thermal, and magnetic
properties [2, 3].
Thin-film samples of the Fe
86
Mn
13
C alloy can be
used as materials for spintronics.
The aim of this work was to investigate features of
martensite transformation and the magnetic structure
formed during plastic deformation in bulk and thin-
film alloy samples.
EXPERIMENTAL
Thin discs of Fe
86
Mn
13
C alloy, cut from bulk sam-
ples using the electric spark method, were thinned by
jet polishing.
Films of the same alloy were obtained via thermal
deposition on NaCl substrates and coating glass at a
rarefaction of 10
–5
mm Hg in a VUP-4 vacuum instal-
lation.
Internal stresses and deformations in film and bulk
samples were induced through their multiple immer-
sion into liquid nitrogen, due to the strong tempera-
ture gradient.
Thinned bulk and film samples were investigated
via electron microscopy on JEOL-2010, JEOL-2100,
and EM-200 electron microscopes. Lorenz contrast
was obtained in the EM-200 electron microscope in
the mode of an active and inactive objective lens.
RESULTS AND DISCUSSION
Figure 1 shows the electron microscopy image of a
thin disc of Fe
86
Mn
13
C alloy subjected to cryomechan-
ical treatment in liquid nitrogen. Localization plastic
deformation zones ~1 nanometer thick can be seen.
Similar plastic deformation zones were discussed in
[4], where a schematic of the reorientation of nanos-
trips in a nickel submicrocrystal after torsion plastic
Investigating Deformation Martensite in Thinned Samples
and Films of Fe
86
Mn
13
C Alloy
R. B. Abylkalykova
a
, A. V. Dzhes
b
, L. I. Kveglis
c
, F. M. Noskov
c
,
M. N. Volochaev
d
, and A. G. Cherkov
e
a
East Kazakhstan State University, Ust’-Kamenogorsk, 070020 Kazakhstan
b
East Kazakhstan State Technical University, Ust’-Kamenogorsk, 070004 Kazakhstan
c
Siberian Federal University, Krasnoyarsk, 660041 Russia
d
Siberian State Aerospace University, Krasnoyarsk, 660014 Russia
e
National Research University, Novosibirsk, 630090 Russia
e-mail: kveglis@iph.krasn.ru
Abstract—The structure and properties of film and bulk samples of Fe
86
Mn
13
C alloy are investigated exper-
imentally. The formation of the deformation martensite structure in Fe
86
Mn
13
C alloy is described in terms of
cluster models of FCC and BCC structures.
DOI: 10.3103/S1062873814040030
10 nm
Fig. 1. Electron microscopy high-resolution image of a
thinned sample of Fe
86
Mn
13
C alloy subjected to cryome-
chanical treatment.