Journal Pre-proof Experimental protocol for the study of One-pot amination of Cyclohexanone-to-Secondary amines over Carbon-supported Pd Luis E. Arteaga-P ´ erez , Raydel Manrique , Francisca Castillo-Puchi , Maray Ortega , Camila Bertiola , Romel Jim ´ enez , Andy J. P´ erez PII: S1385-8947(21)00825-1 DOI: https://doi.org/10.1016/j.mex.2021.101406 Reference: MEX 101406 To appear in: MethodsX Received date: 8 March 2021 Accepted date: 31 May 2021 Please cite this article as: Luis E. Arteaga-P ´ erez , Raydel Manrique , Francisca Castillo-Puchi , Maray Ortega , Camila Bertiola , Romel Jim ´ enez , Andy J. P ´ erez , Experimental protocol for the study of One-pot amination of Cyclohexanone-to-Secondary amines over Carbon-supported Pd, Meth- odsX (2021), doi: https://doi.org/10.1016/j.mex.2021.101406 This is a PDF ﬁle of an article that has undergone enhancements after acceptance, such as the addition of a cover page and metadata, and formatting for readability, but it is not yet the deﬁnitive version of record. This version will undergo additional copyediting, typesetting and review before it is published in its ﬁnal form, but we are providing this version to give early visibility of the article. Please note that, during the production process, errors may be discovered which could affect the content, and all legal disclaimers that apply to the journal pertain. © 2021 Published by Elsevier B.V. This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/)