Volume 5 • Issue 6 • 1000216
J Textile Sci Eng
ISSN: 2165-8064 JTESE, an open access journal
Research Article Open Access
Eyupoglu et al., J Textile Sci Eng 2015, 5:6
DOI: 10.4172/2165-8064.1000216
Research Article Open Access
ISSN: 2165-8064
Abstract
In this study, oxygen and nitrogen plasma treatment was carried out on wool fabrics during 5, 10 and 15 minutes
at low (LF) (40 kHz) and radio (RF) (13.59 MHz) frequency. Then the effect of plasma treatment on tear strength,
contact angle, whiteness and yellowness index of wool fabrics was investigated. In addition, the hydrophility of
plasma treated samples was analyzed after the washing. The physical and chemical properties of wool fabrics
treated with oxygen and nitrogen plasma were characterized by scanning electron microscope (SEM) and energy
dispersive X-ray spectroscopy (EDX). According to the results, nitrogen plasma treatment improved the tear strength
of samples. Furthermore, plasma treatment increased the yellowness of samples while decreasing the whiteness
index of samples. The hydrophility of samples decreases with plasma treatment and with the increase in plasma
treatment time. Moreover, SEM results showed that the plasma treatment caused to occur deformations on the
surfaces. Lastly, EDX results showed that the amount of oxygen and nitrogen increased in the surfaces after oxygen
and nitrogen plasma treatment.
Investigation of the Effect of Different Plasma Treatment Condition on the
Properties of Wool Fabrics
Eyupoglu S
1
*, Kilinc M
1
and Kut D
2
1
Engineering and Design Faculty, Department of Fashion and Textile Design, Istanbul Commerce University, Istanbul, Turkey
2
Engineering Faculty, Department of Textile Engineering, Uludag University, Bursa, Turkey
*Corresponding author: Seyda Eyupoglu, Faculty of Engineering and Design,
Department of Fashion and Textile Design, Istanbul Commerce University,
Kucukyali E5 Crossroad, Istanbul 34840, Turkey, Tel: +90 444 0 413-3225; E-mail:
scanbolat@ticaret.edu.tr
Received October 01, 2015; Accepted October 07, 2015; Published October 12,
2015
Citation: Eyupoglu S, Kilinc M, Kut D (2015) Investigation of the Effect of Different
Plasma Treatment Condition on the Properties of Wool Fabrics. J Textile Sci Eng
5: 216. doi:10.4172/2165-8064.1000216
Copyright: © 2015 Eyupoglu S, et al. This is an open-access article distributed
under the terms of the Creative Commons Attribution License, which permits
unrestricted use, distribution, and reproduction in any medium, provided the
original author and source are credited.
Keywords: Oxygen plasma; Nitrogen plasma; Wool; Tear strength;
Hydrophility; Whiteness; Yellowness index
Introduction
In textile industry, wool materials have been used for a long time
because of their high thermal insulation, comfort and eco-friendliness,
while having problems such as felting, pilling, luster and shrinkage [1-
5]. In order to solve these problems, chemical and physical treatments
have been recently used. Some chemical treatments used are ozone,
enzyme and oxidation treatments while plasma treatment, electron
beam irradiation, ion implantation and ultrasonic irradiation are
among physical treatments commonly used [6-9].
Plasma technology has been applied in textile industry in order to
produce a variety of surface modifcations of textile materials. It also
improves a wide range of textile properties such as hydrophobicity,
dye exhaustion, adhesion etc. [10]. Furthermore, the use of plasma
treatment provides more antibacterial, fame retardant, hydrophobic,
hydrophilic, anti-pilling, electric conductivity, anti-static, scouring,
anti-felting, ultraviolet protective textile materials [11-15]. Besides,
plasma technology, characterized by low consumption of water, energy
and chemicals, is a clean, ecologic and dry technique [6,16]. In addition
to these advantages, plasma treatment does not infuence textile
material bulk properties [17,18].
A variety of gases have been used in plasma treatment such as
oxygen, hydrogen, nitrogen and argon [16]. Each gas gives diferent
features to textiles in relation to their chemical groups [19-21].
Te aim of this study is to investigate the efects of plasma
treatment and gas type on wool fabrics without any pre-treatment. In
pre-treatment, wool fabrics were cleaned by Soxhlet extraction with
dichloromethane rinsed with ethanol and deionized water before
the plasma treatment [8]. Tis study difers from the others in that
wool samples were not scoured. In this study, LF and RF oxygen and
nitrogen plasma treatments were performed on wool fabrics for 5,
10 and 15 minutes. Afer the plasma treatment, the efects of plasma
gas, time and frequency of treatment on the wool properties such as
tear strength, hydrophility, whiteness index and yellowness were
investigated. Moreover, the hydrophility of plasma treated samples
was tested to analyze the durability of their hydrophobic properties
afer washing. Te surface of wool fabrics was analyzed by SEM. Te
results demonstrated that nitrogen plasma treatments improved the
tear strength of wool fabrics. Moreover, afer the plasma treatment
yellowness of samples increased and the whiteness index of samples
decreased with the increase in treatment time. Te hydrophility of
samples decreased with the plasma treatment. Te results did not
change afer the washing, as plasma treated samples were hydrophobic.
Material and Methods
Fabrics
In this study, 100% wool plain weave fabric was used to investigate
the diferent efects of plasma treatment on the properties of fabric.
Te fabric specimens were 1:1 plain fabrics (24 ends cm
-1
, 40 Nm; 22
picks cm
-1
, 48 Nm; 40 g/m
2
). Besides the wool fabrics were not cleaned
by Soxhlet extraction with dichloromethane rinsed with ethanol and
deionized water before the plasma treatment.
Plasma treatment
Plasma treatment was performed on wool fabrics with Diener
vacuum plasma with oxygen and nitrogen gas. In this study, the
efects of diferent gases, frequency intensity and plasma treatment
time on wool fabrics were investigated. Wool fabrics were treated with
oxygen and nitrogen plasma for 5, 10 and 15 minutes. Afer a lot of
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ISSN: 2165-8064