Vol.:(0123456789) 1 3
European Food Research and Technology
https://doi.org/10.1007/s00217-019-03364-3
ORIGINAL PAPER
A multipronged favor comparison of Ecuadorian CCN51 and Nacional
cocoa cultivars
Hayley Rottiers
1,2
· Daylan Amelia Tzompa Sosa
1
· Valérie Lemarcq
1
· Ann De Winne
3
· Jocelyn De Wever
2
·
Helena Everaert
1,2
· Julio Andrés Bonilla Jaime
4
· Koen Dewettinck
1
· Kathy Messens
2
Received: 13 June 2019 / Revised: 7 August 2019 / Accepted: 10 August 2019
© Springer-Verlag GmbH Germany, part of Springer Nature 2019
Abstract
Two cocoa types are predominantly being cultivated in Ecuador, the highly appreciated fne Nacional and the high-yielding
and disease-resistant CCN51, classifed as bulk. With the introduction of foreign germplasm in Ecuador and the international
demand for high-quality Nacional cocoa, the present study aims to characterize and compare the favor profle of Nacional
hybrids (EET103, EET559, EET576 and EET577) and CCN51, and to assess the efect of the genotype. The fermented dried
beans were processed into liquor and their sensory properties, volatile composition and odor fngerprint were analyzed by
trained panelists, headspace–solid phase microextraction gas chromatography–mass spectrometry (HS–SPME–GC–MS),
and GC electronic nose (e-nose), respectively, combined with multivariate statistics. Seventy volatiles were identifed and
semi-quantifed, among them, 16 and 14 volatiles conferring fruity and foral aroma notes, respectively. CCN51 was mainly
characterized by undesirable odor-active volatiles, whereas the EET cultivars contained the highest concentration of most
fruity and foral volatiles, with diferences in between EET cultivars. Sensory data highlighted organoleptic diferences
between the fne and bulk liquors, i.e. the fruity and acid EET favor strongly difered from the bitter, astringent and of-favor
attributes of CCN51. Principal component analysis (PCA) discriminated frstly between fne and bulk, and secondly between
EET identity. Partial least squares analysis identifed possible correlations between sensory attributes and volatile compounds.
Besides, e-nose proved its usefulness for rapid assessment of the liquors’ sensory profle. The results provide a foundation
for understanding the genotype’s contribution to and the compositional basis of Ecuadorian fne and bulk cocoa favor.
Keywords Cocoa liquor · Fine and bulk · Aroma profle · Sensory evaluation · GC e-nose
Abbreviations
A.S.S.(P.)S. Arriba Superior Summer (Plantación)
Selecto
CCAT Centro de Cacao Aroma Tenguel
E-nose Electronic nose
EET-P Estación Experimental Tropical Pichilingue
FI Fermentation index
FID Flame ionization detector
GC–MS Gas chromatography–mass spectrometry
HS Headspace
INEN Servicio Ecuatoriano de Normalización
ISO International Organization for
Standardization
KI Kovat indices
NTE Norma Técnica Ecuatoriana
Electronic supplementary material The online version of this
article (https://doi.org/10.1007/s00217-019-03364-3) contains
supplementary material, which is available to authorized users.
* Hayley Rottiers
hayley.rottiers@ugent.be
1
Laboratory of Food Technology and Engineering (FTE),
Department of Food Technology, Safety and Health, Faculty
of Bioscience Engineering, Ghent University, Ghent,
Belgium
2
Research Group Molecular Biotechnology (MOBI),
Department of Biotechnology, Faculty of Bioscience
Engineering, Ghent University, Ghent, Belgium
3
Center for Aroma and Flavour Technology, Department
of Microbial and Molecular Systems (M²S), Cluster
Bioengineering Technology, KU Leuven Technology
Campus Ghent, Ghent, Belgium
4
Escuela Superior Politécnica del Litoral (ESPOL), Centro
de Investigaciones Biotecnológicas del Ecuador (CIBE),
Facultad de Ciencias de la Vida, Campus Gustavo Galindo
Km. 30.5 Vía Perimetral, P.O. Box 09-01-5863, Guayaquil,
Ecuador