Utilization of Pistia stratiotes (aquatic weed) for fermentative biohydrogen: Electron-equivalent balance, stoichiometry, and cost estimation Nonsikelelo Precios Mthethwa a , Mahmoud Nasr b , Faizal Bux a , Sheena Kumari a,* a Institute for Water and Wastewater Technology, Durban University of Technology, Durban 4000, South Africa b Sanitary Engineering Department, Faculty of Engineering, Alexandria University, Alexandria 21544, Egypt article info Article history: Received 14 January 2018 Received in revised form 13 March 2018 Accepted 15 March 2018 Available online xxx Keywords: Bacterial community Biohydrogen cost Dark-fermentation Full stoichiometry Pistia stratiotes substrate abstract This study investigated the utilization of Pistia stratiotes for biohydrogen production via a dark-fermentation process. The aquatic plant was subjected to acid-hydrolysis using H 2 SO 4 : 3.0% (v/v) for 40 min, resulting in sugar yield: 122.2 ± 5.2 mg/g. The optimum culture pH was 5.5, achieving hydrogen yield (HY): 2.46 ± 0.14 mol-H 2 /mol-glucose (3.51 ± 0.20 mg-H 2 /g-dry weight) at fermentation time 8 h, temperature 25 C, and substrate-to-biomass (S/X) ratio 1.0 g-COD/g-VSS. The organic mass balance (92e96%) and electron-equivalent balance (92e98%) indicated the reliability of fermentation data. The dominant species included Planctomycetales, Verrucomicrobiales, Clostridiaceae, and Gammaproteobacteria. The phyloge- netic analysis confirmed the abundance of hydrogen-producing bacteria such as Bacillus, Clostridium, and Enterobacter. The hydrogenase gene expression provided the highest activity at pH: 5.5 with a cell number 2.53 10 4 copies/ng-DNA compared to pH: 4.5 (6.95 10 3 copies/ng-DNA) and pH: 8.5 (7.77 10 3 copies/ng-DNA). The total cost of the fermentation system including the amortization cost of investment and operating cost was 0.08 $/kg-dry weight (22.8 $/kg-H 2 produced). © 2018 Hydrogen Energy Publications LLC. Published by Elsevier Ltd. All rights reserved. Introduction Hydrogen gas (H 2 ) is considered as a potential green energy carrier that can meet the increasing global energy demand [1]. H 2 has a higher energy content per unit weight (122e142 kJ/g) compared to other fossil fuels such as coal, petroleum, oil, and natural gas [2].H 2 produces only H 2 O during combustion [3] and can be utilized in fuel cells and vehicle engines [4].H 2 can be generated by various methods such as steam reform- ing, photoelectrochemical, photocatalytic, electrolysis, and thermolysis [5]. However, many of these techniques employ high quantities of heavy oil and fossil materials that increase the energy input and cause environmental deterioration [6]. Biological fermentation is an efficient and environmentally friendly method for H 2 production as it can be conducted under ambient operating temperature and atmospheric pressure [7]. In this process, microorganisms ferment substrate in the form of wastewater or biomass [8]. This trend results in achieving net positive energy (i.e., producing hydrogen), and in parallel, solving pollution problems (i.e., wastes removal) [9]. Dark- and photo-fermentations are the main biological routes of H 2 gen- eration [10]. In dark-fermentation, hydrogen-producing mi- croorganisms utilize carbohydrate-rich substrates under an * Corresponding author. E-mail address: sheenas@dut.ac.za (S. Kumari). Available online at www.sciencedirect.com ScienceDirect journal homepage: www.elsevier.com/locate/he international journal of hydrogen energy xxx (2018) 1 e13 https://doi.org/10.1016/j.ijhydene.2018.03.099 0360-3199/© 2018 Hydrogen Energy Publications LLC. Published by Elsevier Ltd. All rights reserved. Please cite this article in press as: Mthethwa NP, et al., Utilization of Pistia stratiotes (aquatic weed) for fermentative biohydrogen: Electron-equivalent balance, stoichiometry, and cost estimation, International Journal of Hydrogen Energy (2018), https://doi.org/ 10.1016/j.ijhydene.2018.03.099