1 Direct observation of transitions between surface- dominated and bulk diffusion regimes in nanochannels Nicolas F.Y. Durand, *† Claudio Dellagiacoma, § Raphaël Goetschmann, Arnaud Bertsch, Iwan Märki, § Theo Lasser, § and Philippe Renaud Microsystems Laboratory and Biomedical Optics Laboratory, Swiss Federal Institute of Technology (EPFL), Lausanne, Switzerland * To whom correspondence should be addressed. E-mail: nicolas.durand@epfl.ch Microsystems Laboratory § Biomedical Optics Laboratory These authors contributed equally to this work.