1 3
J Biol Inorg Chem
DOI 10.1007/s00775-016-1428-x
ORIGINAL PAPER
EPR interpretation, magnetism and biological study of a Cu(II)
dinuclear complex assisted by a schiff base precursor
Kuheli Das
1,2
· Chiranjit Patra
1
· Chandana Sen
1
· Amitabha Datta
2
· Chiara Massera
3
· Eugenio Garribba
4
·
Mohamed Salah El Fallah
5
· Belete B. Beyene
2
· Chen-Hsiung Hung
2
· Chittaranjan Sinha
1
· Tulin Askun
6
·
Pinar Celikboyun
6
· Daniel Escudero
7
· Antonio Frontera
8
Received: 9 August 2016 / Accepted: 6 December 2016
© SBIC 2016
complex by DFT computation. Both the ligand and complex
1 exhibit anti-mycobacterial activity and considerable effi-
cacy on M. tuberculosis H
37
Ra (ATCC 25177) and M. tuber-
culosis H
37
Rv (ATCC 25618) strains. The practical appli-
cability of the ligand and complex 1 has been examined in
living cells (African Monkey Vero Cells). The MTT assay
proves the non-toxicity of the probe up to 100 mg mL
-1
.
Graphical abstract A new homometallic dinuclear Cu(II)
complex is afforded with a tetradentate Schiff base precur-
sor. EPR interpretation and temperature dependent mag-
netic studies show that complex 1 has weak antiferromag-
netic coupling and DFT computation is governed to explain
the magneto-structural correlation.
Abstract A new Cu(II) dinuclear complex, Cu
2
L
2
(1) was
afforded employing the potentially pentatentate Schiff base
precursor H
2
L, a refluxed product of o-vanillin and dieth-
ylenetriamine in methanol. Complex 1 was systematically
characterized by FTIR, UV–Vis, emission and EPR spec-
trometry. The single crystal X-ray diffraction analysis of
1 reveals that the copper atom exhibits a distorted square
planar geometry, comprising two pairs of phenolato-O and
imine-N donors from two different H
2
L ligands. The tem-
perature dependent magnetic interpretation agrees with the
existence of weak antiferromagnetic interactions between
the bridging dinuclear Cu(II) ions. A considerable body of
experimental evidence has been accumulated to elucidate
the magneto-structural relationship in this dinuclear Cu(II)
Electronic supplementary material The online version of this
article (doi:10.1007/s00775-016-1428-x) contains supplementary
material, which is available to authorized users.
* Amitabha Datta
amitd_ju@yahoo.co.in
* Chen-Hsiung Hung
chhung@gate.sinica.edu.tw
* Chittaranjan Sinha
c_r_sinha@yahoo.com
1
Department of Chemistry, Jadavpur University,
Kolkata 700032, India
2
Institute of Chemistry, Academia Sinica, Nankang,
Taipei 115, Taiwan
3
Dipartimento di Chimica, Universita degli Studi di Parma,
Viale delle Scienze, 17/A, 43124 Parma, Italy
4
Dipartimento di Chimica e Farmacia, Università di Sassari,
Via Vienna 2, 07100 Sassari, Italy
5
Departament de Química Inorgànica, Facultat de
Química, Universitat de Barcelona, Martíi Franquès, 1-11,
08028 Barcelona, Catalunya, Spain
6
Department of Biology, Faculty of Sciences and Arts,
University of Balikesir, Cagis Campus, 10145 Balıkesir,
Turkey
7
CEISAM UMR CNRS 6230, Université de Nantes, 2 rue de
la Houssinière, BP 92208, 44322 Nantes Cedex 3, France
8
Departament de Quimica, Universitat de les Illes Balears,
Crta. de Valldemossa km 7.5, 07122 Palma de Mallorca
(Baleares), Spain