Effects of Drying Temperatures and Glycerol
Concentrations on Properties of Edible Film from
Konjac Flour
Lamul Wiset
1
, Nattapol Poomsa-ad
2
, and Prayoon Jomlapeeratikul
3
Faculty of Engineering/Mahasarakham University, Mahasarakham, Thailand
Email: {
1
Lamulwiset,
3
prayoon_eng}@hotmail.com;
2
nattapol.p@msu.ac.th
Chaleeda Borompichaichartkul
Faculty of Science, Chulalongkorn University, Bangkok, Thailand
Email: chaleedab@hotmail.com
Abstract—The objective of this research was to study the
effect of drying temperatures and glycerol concentrations on
properties of edible film from konjac flour. Glycerol was
used as plasticizer at the concentrations of 0 and 0.3% w/v
for film forming. The drying process was done using heat
pump dryer at various temperatures of 45, 50 and 55 C.
Sample was dried until the final moisture content was down
to 1% wet basis. Then, film samples were taken to
determine various properties including, tensile strength,
elongation, water vapor permeability and solubility. The
results found that konjac film without glycerol had a higher
tensile strength than that konjac film with 0.3% glycerol.
Also, tensile strength was significantly increased with the
increasing of drying temperature (p ≤ 0.05). For the
elongation, water vapor permeability and solubility of film,
these properties of konjac film with 0.3% glycerol were
higher than that konjac film without glycerol. The
elongation was significantly decreased when the drying
temperature increased (p ≤ 0.05). Moreover, water vapor
permeability and solubility were significantly difference at
various drying temperature (p ≤ 0.05). The drying
temperature at 50 C provided the lowest water vapor
permeability and the highest solubility
Index Terms—edible film, konjac, drying, plasticizer, film
properties
I. INTRODUCTION
The wide use of petroleum-derived plastics and the
negative impact of these on the environment prompted
the search for biodegradable materials obtained from
renewable resources. The use of agriculture derived
biopolymers, such as proteins and glucomannan, appears
as an interesting alternative to synthetic plastics for some
applications, especially those with a short life-time, such
as food packaging, and generates new uses of higher
added value for agriculture products [1].
Edible films and coatings have long been used to
protect food products, improving food quality. The
application of edible films is a technological hurdle that
Manuscript received August 31, 2013; revised November 2, 2013.
can modify vegetable tissue metabolism while affecting
respiration; they can be conveyors of antimicrobials,
antioxidants and other preservatives; they can enrich
product formulation, carrying vitamins and minerals [2].
In general, edible films and coatings provide the potential
to control transport of moisture, oxygen, aroma, oil, and
flavor compounds in food systems, depending on the
nature of the edible film-forming materials [3]. The
physical and mechanical properties of edible films are a
subject of great importance due to their influence on
product performance and consumer acceptance.
Konjac glucomannan (KGM) is the main renewable
products which are economical, readily available,
biodegradable and highly safe. They possess special
nutritional and/or health-protective functions as well as
good film-forming properties. For instance, KGM is
found to have functions such as has the ability to lower
blood cholesterol and sugar level, help with weight loss,
promote intestinal activity and immune function [4].
One important component of edible films is the
plasticizer which is required to overcome film brittleness
and improve its flexibility and extensibility [5].
Plasticizers are low molecular weight components added
to films to reduce their brittleness, by increasing the
space between polymer chains and, consequently,
decreasing the intermolecular attractive forces and
increasing the flexibility and extensibility of the material
[6], [7]. An alternative to reduce the hygroscopicity of
films is the utilization of hydrophobic plasticizers.
The effect of given drying conditions depends on
various characteristics of the raw material, such as a pre-
existing gel phase or the occurrence of thermal gelation
during drying. Moreover, various phenomena, such as the
transition from an amorphous to a vitreous phase, the
appearance of phase separation (thermodynamic
incompatibility) and crystallization, may occur. The
interaction between the physicochemical nature of
biopolymers and the drying conditions is very important
[8].
Banker et al. [9] show that found the water vapor
permeability of cellulose films increased as the film
Journal of Medical and Bioengineering Vol. 3, No. 3, September 2014
171 ©2014 Engineering and Technology Publishing
doi: 10.12720/jomb.3.3.171-174