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Materials Today: Proceedings 5 (2018) 14722–14731 www.materialstoday.com/proceedings
2214-7853 © 2017 Elsevier Ltd. All rights reserved.
Selection and/or Peer-review under responsibility of Extended Defects In Semiconductors 2016 (EDS 2016).
EDS 2016
Strain buildup in 4H-SiC implanted with noble gases at low dose
C. Jiang, L. Dagault, V. Audurier, C. Tromas, A. Declémy, M.-F. Beaufort and
J.-F. Barbot*
Pprime Institut, département Physique et Mécanique des Matériaux, CNRS-Université de Poitiers-ENSMA, BP 30179, 86962 Futuroscope-
Chasseneuil Cedex 05, France
Abstract
4H-SiC single crystals were implanted at room temperature (RT) and at 673 K with different noble gases in a low dose regime.
Strain buildup has been systematically investigated based on X-ray diffraction analysis. At RT the strain increase with dose is
linear up to amorphization. With increasing temperature, 673 K, the accumulation shows a two-step shape. The first step can be
anticipated by using the direct impact model independent of incident ions. Beyond a critical dose, a second step of strain is
observed with an accumulation scenario related to the creation of defects, cascade overlapping and their enhanced stability via
their interaction with gas. At low dose, the strain recovery under annealing is a thermally activated process whose underlined
mechanisms are similar to those of dynamic recovery. Moreover, the surface swelling is closely related to this implantation-
induced elastic strain. At RT, the hardening effect of about 10% has been confirmed at low dose. The increase of fracture
toughness as well as hardness changes under implantation seems to be related to the increase of the in-plane stresses and to the
nucleation/ pinning of dislocation via the generation of point-like defects.
© 2017 Elsevier Ltd. All rights reserved.
Selection and/or Peer-review under responsibility of Extended Defects In Semiconductors 2016 (EDS 2016).
Keywords: ion implantation, strain, SiC, mechanical properties
1. Introduction
Silicon Carbide (SiC) gains interests as a wide bandgap semiconductor material due to its attractive chemical,
physical, and electronic properties for high-power, high-temperature, and high-frequency electronic devices; the
more dominant polytype being 4H-SiC. Ion implantation is the only viable technology for a selective area doping of
* Corresponding author. Tel.: +33-549-496-734; fax: +33-549-496-692.
E-mail address: jean.francois.barbot@univ-poitiers.fr