ISSN 0147-6874, Moscow University Soil Science Bulletin, 2010, Vol. 65, No. 4, pp. 179–182. © Allerton Press, Inc., 2010.
Original Russian Text © M.A. Timofeev, V.A. Terechova, P.A. Kozhevin, 2010, published in Vestnik Moskovskogo Universiteta. Pochvovedenie, 2010, No. 4, pp. 44–47.
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INTRODUCTION
Great importance in environmental ecological
monitoring is attributed to biotic indicators. They
contain unique information that cannot be collected
using physical and chemical tests alone. In particular,
chemical analysis reveals the presence of pollutants,
but, given its understandable limitations, it cannot
provide an unambiguous characterization of the con-
dition of soil biota and the ecosystem generally, or pre-
dict future events. Biotesting techniques allow one to
make an integral assessment of ecological hazard lev-
els [17].
The main principle of biotesting lies in determining
the action of environmental samples on biological test
specimens, which allows one to determine the integral
biological effects of the totality of adverse environ-
mental factors [13]. Special studies are required to
understand the technique’s capabilities and limita-
tions, especially when the observed reactions of test
subjects reflect the action of other factors than only
pollutants, in situ. Such situations are typical in the
analysis of soil as a complex heterogeneous system.
The development of a biotesting system allowing one
to not only ascertain the fact of contamination, but
also to obtain qualitative and quantitative characteris-
tics is no less topical [13]. In order to solve such prob-
lems, analysis utilizing the methods of multidimen-
sional mathematical statistics is called for [1].
Microbiological testing techniques, including pol-
lution-induced community tolerance of microorgan-
isms (PICT) are of especial interest for obtaining the
qualitative and quantitative characteristics of contam-
ination [14]. In this case, communities in soil samples
themselves, rather than individual organisms and pop-
ulations, play the role of test subjects [4].
In this work, the range of biosystems that are suit-
able for the efficient ecotoxicological assessment of
soil samples in soils has been determined based on the
example of cadmium pollution.
EXPERIMENTAL
This study was conducted on sod–podzol soil
(from the Moscow oblast) and modal chernozem
(from the Tula oblast) samples collected from the top
(0–20 cm) horizons, as well as on model soil mixture
samples having the following composition: terrestrial
peat (10%), kaolin clay (20%), and quartz sand (70%)
(as per ISO 11268-1).
At the first stage, physical and chemical techniques
were used on the soils and model mixture to determine
the acidic and basic properties and assay organic mat-
ter, mobile phosphorus, as well as potassium com-
pounds and silt.
In the main experiment, cadmium chloride solu-
tions were introduced into soil and model mixture
samples at two levels: 25 and 250 mg/kg of soil
(10 and 100 threshold limit values (TLV), respec-
tively), and the samples were subsequently moistur-
ized (0.005 MPa). They were thoroughly mixed to
ensure even distribution of the toxicant [16].
Incubation was carried out in a thermostat at 25°C.
Samples for analysis were collected 7 and 30 days after
the introduction of cadmium. The 1st week was pre-
sumed to be a period of acute toxicity with probable
inhibition of microbial growth. Prolonged incubation
for 1 month was designed to test the possibility of in situ
formation of pollution-resistant microbial populations.
Eleven biological techniques were used for ecolog-
ical assessment. Six of these are biotesting systems; the
test organisms included Raphanus sativa radish seeds
(three-day germination power test; 7-day germination
capacity, specific length and sprout biomass test) [11];
crustaceans Ceriodaphnia affinis (48-hour immobili-
zation test) [8]; microscopic algae Scenedesmus quad-
ricauda (72-hour population growth inhibition test)
[6]; an in vitro homoiothermal animal cell culture
(3-hour express test based on the change in the motil-
ity of bovine sperm cells) [5]; Paramecium caudatum
(24-hour immobilization test) [9]; and luminescent
biosensor Ecolum (30-minute bacterial luminescence
Biotesting for Cd Pollution in Soils
M. A. Timofeev, V. A. Terechova, and P. A. Kozhevin
Received May 11, 2010
Abstract—The potential of biotesting to detect and analyze Cd pollution in soils was studied. This paper
identifies a number of approaches, such as PICT and discriminant analysis, which may open new perspectives
for ecotoxicology.
Keywords: cadmium, soil pollution, biotesting, ecotoxicology.
DOI: 10.3103/S0147687410040095