International Journal of Engineering Research and Technology. ISSN 0974-3154, Volume 13, Number 12 (2020), pp. 4156-4162
© International Research Publication House. http://www.irphouse.com
4156
Dynamic Shear Rheometer to Measure the Improvement of Asphalt
Properties with the Addition of Buton Natural Asphalt-Rubber (BNA-R)
Sigit Pranowo Hadiwardoyo
1,*
, R. Jachrizal Sumabrata
2
, Nurul Wahjuningsih
3
Department of Civil Engineering, Faculty of Engineering, Universitas Indonesia, Depok 16242, Indonesia.
ORCID:
1)
0000-0001-8734-4794;
2)
0000-0003-3668-4734,
3)
0000-0003-4587-7490
Abstract
The characteristic of asphalt was influenced from temperature
and load. Modifications of the characteristics of asphalt can
improve their performance. Changes to the complex shear
modulus will affect the stiffness modulus of asphalt. Indonesia
has considerable deposits of natural asphalt, namely Buton
natural asphalt, which has the potential to be used as an
asphalt modifier. Buton natural asphalt-rubber (BNA-R) is
one of the products of Buton natural asphalt mixed with
rubber. This study uses a dynamic shear rheometer (DSR) to
examine the effects of BNA-R on the rheology of virgin
asphalt. Tests were carried out on samples before and after
aging. The added quantity of BNA-R was varied from 2.5 %
to 20 % with respect to Pen 64.2 virgin asphalt. The addition
of BNA-R increased the hardness and improved the
rheological properties of asphalt by increasing its performance
grade (PG) and complex shear modulus (G*). The black
diagram and master curve analysis show that the phase angle
value (δ) decreases with the addition of BNA-R and increases
the resistance to temperature.
Keywords: Modified Asphalt, Stiffness Modulus, Complex
Shear Modulus, Buton Asphalt Rubber, Temperature
I. INTRODUCTION
Asphalt or bitumen is one of the oldest building materials and
has been used extensively since ancient times. Initially,
natural asphalt was processed at high temperatures to remove
oil fractions and maintain high molar mass. Asphalt materials
show thermoplastic properties and because of their superiority
to water and their adhesive properties, they are used in various
applications. Currently, asphalt is produced from crude oil via
distillation, where an increase in temperature reduces the
volatile-component content. Bitumen is a complex
hydrocarbon which is regarded as a colloidal system
consisting of high molecular weight asphaltenes dispersed in a
lower molecular weight maltenes [1], [2].
Deposits of natural rock asphalt in Indonesia is found on
Buton Island; the material is also known as Asbuton. There is
a massive reserve of natural rock asphalt with a 5-30 %
asphalt content and the estimated deposit amount is up to 677
million tons [3]. Asbuton has a great chance of being used
partially or completely as a substitute for asphalt oil in asphalt
mixtures. Asbuton is produced by extracting Buton rock
asphalt and is more widely used as a modifier or added
material because its penetration is extremely low [4]. Buton
natural asphalt-rubber (BNA-R) is a mixture of Buton rock
asphalt and crumb rubber. BNA-R contains 60 % asphalt as a
result of semi-extraction from Buton rock asphalt and 40 %
crumb rubber and has several advantages such as high
stickiness, high softening point, high stiffness modulus, high
resistance to fracture, and a durable and economical value [5],
[6].
A mixture of asphalt and aggregates produces a heterogeneous
material, generally consisting of original or used aggregates
(recycled from industrial processes or otherwise), an asphalt
binder, and air cavities. The mechanical properties of
aggregate asphalt mixtures are mainly influenced by the
nature of the asphalt. In general, aggregate asphalt mixtures
show a time-dependent behavior with a characteristic
nonlinear visco elastic stress-strain response (except under
very low stresses or strains) [7].
As a thermoplastic material, asphalt has visco elastic
properties under the conditions of most pavement operations.
These properties determine the behavior of asphalt mixtures,
usually measured by the relationship between stress and strain.
The rheological properties of asphalt are usually presented in
the form of complex shear modulus curves (G*) and phase
angles (δ). G* is defined as the ratio of maximum stress (shear)
to maximum strain when experiencing shear loads. δ is the
phase difference between the voltage and strain in harmonic
oscillation. Furthermore, the master curve helps to understand
the behavior of asphalt binders for various loading frequencies
under different temperature conditions. The main laboratory
equipment for obtaining these parameters is a dynamic shear
rheometer (DSR). Even at low temperature, the DSR still
suitable to investigate the rheological properties of bitumen
[8]–[13].
One of the most common flexible pavement damage in high-
temperature countries such as Indonesia is rutting. The
Superpave rutting factor (G*/Sin δ) has been used to evaluat e
the potential resistance to rutting of asphalt at high
temperatures [11]. Other researchers call this value an anti-
rutting factor [8], [14]–[18]. G*/Sin δ is derived from the
dissipation energy concept (ΔU) (AASHTO T315-15). The
ΔU value for the loading cycle can be calculated using Eq. (1)
[11].
∆ =
(1)
where ε max is the maximum shear strain, σ max is the
maximum shear stress, and δ is the phase angle. Under stress