[149] CODEN (CAS-USA): WJCMCF
Formulation and evaluation of oral disintegrating tablets of furosemide
Manish Khadka*
1
, Dharma Prasad Khanal
1
, Deepti Piya Baniya
1
, Prakash Karki
1
and Saurav Shrestha
2
1
Department of Pharmacy, Manmohan Memorial Institute of Health Sciences, Tribhuvan University, Soalteemode-44600,
Kathmandu, Nepal
2
Department of Pharmacy, Institute of Medicine, Maharajgunj Medical Campus, Tribhuvan University, Maharajgunj-44600,
Kathmandu, Nepal
Abstract
Orally disintegrating tablets of Furosemide were prepared, evaluated and the comparison of the action of different concentrations of
disintegrants on disintegration and dissolution of the tablets were studied. Direct compression method was used to prepare the
orally disintegrating tablets containing 20 mg of Furosemide. The formulation was conducted using different concentrations of
crospovidone, croscarmellose and sodium starch glycolate as superdisintegrants and their interactions with Furosemide were also
evaluated using FTIR. FTIR studies using the drug and its mixtures with the excipients showed that the peaks correlate with one
another which signify that there is no interaction between the drug molecule and the excipients used. The obtained results revealed
that the disintegration time of ODTs were between 9 to 59 seconds. The percentage drug content of tablets in all the formulations
was found between 91.51% to 106.69%, which complies with the limits established in pharmacopoeia. The in-vitro dissolution
studies show maximum release of 89.47% in formulation F3 and minimum of 77.64% in formulation F12. Higher concentration of
crospovidone and croscarmellose in formulations F3 and F6 showed better dissolution properties than SSG. So by varying the
concentrations of super disintegrants, oral disintegrating tablets can be formulated.
Introduction
Orally disintegrating tablets are the dosage forms that get
disintegrated when they come in contact with the saliva
present in the oral cavity. The saliva penetrates the tablets and
disrupts its structural integrity which results in the release of
the drug from the dosage form [1]. The rapid disintegration of
the tablets in the oral cavity may be rendered by the use of
super disintegrants, such as crospovidone, croscarmellose and
sodium starch glycolate, thus making the dosage form
favorable for the pediatric population, geriatric population,
bed-ridden patients and patients with dysphagia [2]. According
to the United States Food and Drug Administration, an Oral
Disintegrating Tablet is defined as “A solid dosage form which
contains a medicinal substance or an active ingredient which
rapidly disintegrates when placed upon the tongue, usually
within matter of seconds [3]. The names such as rapid
dissolving, mouth dissolving and fast melt tablets has also been
given to the orally disintegrating tablets. The orally
disintegrating tablets disperse and disintegrate when they
come in contact with the saliva present in the oral cavity that
omits the use of liquid to take the tablet, to swallow the whole
dosage form or to chew the tablet. This dosage form is thus
beneficial to the pediatric and geriatric patients and also to
those who have swallowing difficulties including dysphagia and
patients with psychiatric disorders [4]. Furosemide is a loop
diuretic or often called as a high ceiling diuretic used in the
treatment of edematous states which prevents and treats the
fluid retention in the body. The usual dosage forms of
furosemide available are 20 and 40 mg tablets. Chemically
Furosemide is 5-(aminosulphonyl)-4-chloro-2-[(2-fuanyl-
methyl) amino] benzoic acid [5]. The Biopharmaceutics
Classification System (BCS) classifies furosemide as a Class IV
compound, which means that furosemide has a low solubility
and a low permeability. The bioavailability of furosemide is
found to be 37-70% with its peak plasma concentration (Cmax)
found to be achieved within 60 to 90 min. The plasma half-life
(t1/2) of furosemide is 1.3±0.8 h in healthy subjects [6]. The
purpose of this study is to formulate the ODTs of Furosemide
and to perform the evaluation of those formulations for
different parameters. The use of the superdisintegrants i.e.
Crosspovidone, Croscarmellose sodium and Sodium starch
glycolate and their effects on the tablets’ disintegration and
dissolution has been studied.
Materials and Methods
Raw materials were obtained with coordination with the
Department of Pharmacy MMIHS and Lomus and Qmed
Pharmaceuticals. Furosemide, MCC, sucralose and mannitol
WORLD JOURNAL OF CURRENT MEDICAL AND
PHARMACEUTICAL RESEARCH
www.wjcmpr.com ISSN: 2582-0222
Article History:
Received: 03.10.2021
Revised: 24.10.2021
Accepted: 02.12.2021
Keywords:
Orally disintegrating tablet,
Superdisintegrants, Furosemide, FTIR.
*Corresponding Author
Manish Khadka
Email: maness.kdk@gmail.com
DOI: https://doi.org/10.37022/wjcmpr.v3i6.202
This article is licensed under a Creative Commons Attribution-Non-commercial 4.0 International License.
Copyright © 2021 Author(s) retain the copyright of this article.
World J Curr Med Pharm Res. 2021; 3(6): 149-156
Research Article