Materials Sciences and Applications, 2019, 10, 105-117
http://www.scirp.org/journal/msa
ISSN Online: 2153-1188
ISSN Print: 2153-117X
DOI: 10.4236/msa.2019.102009 Jan. 29, 2019 105 Materials Sciences and Applications
Gas Phase Activation of Methane Molecule with
Lead Benzene Dication Complex Ion,
[Pb(Benzene)
2
]
2+
Joseph K. Koka
1,2
1
School of Chemistry, University of Nottingham, Nottingham, United Kingdom
2
Department of Chemistry, School of Physical Sciences, University of Cape Coast, Cape Coast, Ghana
Abstract
Motivated by the search for ways of a more efficient usage of the ubiquitous,
and unexploited resources of methane, recent progress in the gas-phase acti-
vation of methane by metal dication complex ion is discussed. The gas phase
theoretical and experimental analysis on [Pb(Benzene)
2
]
2+
was conducted.
The [Pb(Benzene)
2
]
2+
complex ions were prepared using a combination of the
pick-up technique and high energy electron impact, and then held in a cold
ion trap. Excitation with tuneable UV radiation resulted in the formation of
[Pb(Benzene)
2
(H
2
O)]
2+
, [Pb(Benzene)
2
(H
2
O)
2
]
2+
, [Pb(Benzene)]
+
, Pb
+
and
Benzene
+
ions when the experimental results were analysed. The two opti-
mised geometries of [Pb(Benzene)
2
]
2+
namely the C
2V
eclipse and C
2
staggered
were observed. Methane activation of [Pb(Benzene)
2
]
2+
complex ion yielded
[Pb(Benzene)
2
(Me)]
2+
. [Pb(Benzene)
2
(H
2
O)(Me)
2
]
2+
,
[Pb(Benzene)
2
(H
2
O)(Me)]
2+
, [PbBenzene(Me)
3
]
2+
and [Pb(Benzene)(Me)]
2+
.
The PEC calculated binding energy of methane to lead benzene dication
complex ion was approximately 25.45% higher than the value recorded on
DFT calculation. This difference was due to the charge differences on the lead
metal centre. While the actual calculated charge on the Pb metal in the opti-
mised geometry was 1.68 the charge of +2 on the Pb metal was considered in
the PEC calculation.
Keywords
Lead, Benzene, Binding Energy, Methane Activation, Dication Complex Ion,
Density Functional Calculations, Potential Energy Curve
1. Introduction
Methane concentrations had increased globally from 722 parts per billion
How to cite this paper: Koka, J.K. (2019)
Gas Phase Activation of Methane Molecule
with Lead Benzene Dication Complex Ion,
[Pb(Benzene)
2
]
2+
. Materials Sciences and
Applications, 10, 105-117.
https://doi.org/10.4236/msa.2019.102009
Received: November 17, 2018
Accepted: January 26, 2019
Published: January 29, 2019
Copyright © 2019 by author(s) and
Scientific Research Publishing Inc.
This work is licensed under the Creative
Commons Attribution International
License (CC BY 4.0).
http://creativecommons.org/licenses/by/4.0/
Open Access