Citation: Sateriale, D.; Forgione, G.;
De Cristofaro, G.A.; Pagliuca, C.;
Colicchio, R.; Salvatore, P.; Paolucci,
M.; Pagliarulo, C. Antibacterial and
Antibiofilm Efficacy of Thyme
(Thymus vulgaris L.) Essential Oil
against Foodborne Illness Pathogens,
Salmonella enterica subsp. enterica
Serovar Typhimurium and Bacillus
cereus. Antibiotics 2023, 12, 485.
https://doi.org/10.3390/
antibiotics12030485
Academic Editors: Joanna
Kozlowska, Anna Duda-Madej,
Filippo Maggi and Nicholas Dixon
Received: 19 December 2022
Revised: 18 January 2023
Accepted: 27 February 2023
Published: 28 February 2023
Copyright: © 2023 by the authors.
Licensee MDPI, Basel, Switzerland.
This article is an open access article
distributed under the terms and
conditions of the Creative Commons
Attribution (CC BY) license (https://
creativecommons.org/licenses/by/
4.0/).
antibiotics
Article
Antibacterial and Antibiofilm Efficacy of Thyme (Thymus
vulgaris L.) Essential Oil against Foodborne Illness Pathogens,
Salmonella enterica subsp. enterica Serovar Typhimurium and
Bacillus cereus
Daniela Sateriale
1
, Giuseppina Forgione
1
, Giuseppa Anna De Cristofaro
1
, Chiara Pagliuca
2
,
Roberta Colicchio
2
, Paola Salvatore
2,3
, Marina Paolucci
1
and Caterina Pagliarulo
1,
*
1
Department of Science and Technology, University of Sannio, Via F. De Sanctis snc, 82100 Benevento, Italy
2
Department of Molecular Medicine and Medical Biotechnologies, University of Naples Federico II,
Via S. Pansini 5, 80131 Naples, Italy
3
CEINGE-Biotecnologie Avanzate s.c.ar.l., Via G. Salvatore 486, 80145 Naples, Italy
* Correspondence: caterina.pagliarulo@unisannio.it; Tel.: +39-0824-305141
Abstract: Nowadays, the wide spread of foodborne illness and the growing concerns about the
use of synthetic food additives have shifted the focus of researchers towards essential oils (EOs) as
possible antimicrobials and preservatives of natural origin. Thanks to their antimicrobial properties
against pathogenic and food spoilage microorganisms, EOs have shown good potential for use as
alternative food additives, also to counteract biofilm-forming bacterial strains, the spread of which
is considered to be among the main causes of the increase in foodborne illness outbreaks. In this
context, the aim of this study has been to define the antibacterial and antibiofilm profile of thyme
(Thymus vulgaris L.) essential oil (TEO) against widespread foodborne pathogens, Salmonella enterica
subsp. enterica serovar Typhimurium and Bacillus cereus. TEO chemical composition was analyzed
through gas chromatography-mass spectrometry (GC-MS). Preliminary in vitro antibacterial tests
allowed to qualitatively verify TEO efficacy against the tested foodborne pathogens. The subsequent
determination of minimal inhibitory concentration (MIC) and minimal bactericidal concentration
(MBC) values allowed to quantitatively define the bacteriostatic and bactericidal effects of TEO. To
evaluate the ability of essential oils to inhibit biofilm formation, a microplate assay was performed for
the bacterial biofilm biomass measurement. Results suggest that TEO, rich in bioactive compounds,
is able to inhibit the growth of tested foodborne bacteria. In addition, the highlighted in vitro anti-
biofilm properties of TEO suggest the use of this natural agent as a promising food preservative to
counteract biofilm-related infections in the food industry.
Keywords: thyme essential oil; antibacterial agent; antibiofilm activity; natural food preservatives;
foodborne illness pathogens
1. Introduction
Foodborne illness encompasses a wide spectrum of illnesses defined by the WHO’s
Department of Food Safety, Zoonoses and Foodborne Diseases (FOS) as a growing public
health problem worldwide [1]. In recent years, most of the foodborne outbreaks in Eu-
rope and the United States were related to the consumption of contaminated meat and
meat products; fresh processed products of pig meat were the most frequently involved
category, along with chicken meat [2]. Meat and meat products contain essential amino
acids, B-group vitamins, minerals and other nutrients ideal both for human nutrition and
microbial growth [3]. Fresh and transformed meat are rich substrates that strongly support
significant microbial growth, since they have nutrients, pH values and water contents
generally compatible with the growth of a large number and variety of microorganisms [4].
Antibiotics 2023, 12, 485. https://doi.org/10.3390/antibiotics12030485 https://www.mdpi.com/journal/antibiotics