2D
7
Li Ultrafast CT-COSY: a new tool for the rapid measurement of tiny
homonuclear lithium scalar couplings.
G. Hamdoun,
a
B. Gouilleux,
b
M. Sebban,
a
G. Barozzino-Consiglio,
a
A. Harrison-Marchand,
a
P. Giraudeau,
b,c
J.
Maddaluno
a
and H. Oulyadi*
,a
a.
Normandie Univ, UNIROUEN, INSA Rouen, CNRS, COBRA (UMR 6014 & FR 3038), 76000 Rouen, France
b.
CEISAM, UMR CNRS 6230, 2 rue de la Houssinière, 44322 Nantes
c.
Institut Universitaire de France, 1 rue Descartes, 75005, Paris, France
Supporting Information
Experimental Section
Fig. S1: 2D
7
Li UF CT-COSY spectra of a 1 : 1 n-BuLi / MeLi solution as a function of the mixing
time t
mix
.
Fig. S2: 2D
7
Li UF CT-COSY spectra of a 1 : 1 n-BuLi / MeLi solution as a function of the
adiabatic pulse Tp.
Table S1: Lithium 7 T
2
values obtained by a CPMG Sequence at 194 MHz and T = 185 K.
Electronic Supplementary Material (ESI) for ChemComm.
This journal is © The Royal Society of Chemistry 2016