Icarus 300 (2018) 392–410 Contents lists available at ScienceDirect Icarus journal homepage: www.elsevier.com/locate/icarus Spectral reflectance (0.35–2.5 μm) properties of garnets: Implications for remote sensing detection and characterization M.R.M. Izawa a,b,* , E.A. Cloutis a , T. Rhind a , S.A. Mertzman c , Jordan Poitras a , Daniel M. Applin a , P. Mann a a Department of Geography, University of Winnipeg, Winnipeg, MB R3B 2E9, Canada b Institute for Planetary Materials, Okayama University—Misasa, 827 Yamada, Misasa, Tottori 682-0193, Japan c Department of Earth and Environment, Franklin and Marshall College, Lancaster, PA 17604-2615, USA a r t i c l e i n f o Article history: Received 15 April 2017 Revised 9 August 2017 Accepted 5 September 2017 Available online 21 September 2017 Keywords: Reflectance spectroscopy Garnet Remote sensing a b s t r a c t The utility of spectral reflectance for identification of the main end-member garnets: almandine (Fe 2+ 3 Al 2 Si 3 O 12 ), andradite (Ca 3 Fe 3+ 2 Si 3 O 12 ), grossular (Ca 3 Al 2 Si 3 O 12 ), pyrope (Mg 3 Al 2 Si 3 O 12 ), spessartine (Mn 2+ 3 Al 2 Si 3 O 12 ), and uvarovite (Ca 3 Cr 3+ 2 Si 3 O 12 ) was studied using a suite of 60 garnet samples. Com- positional and structural data for the samples, along with previous studies, were used to elucidate the mechanisms that control their spectral reflectance properties. Various cation substitutions result in dif- ferent spectral properties that can be determine the presence of various optically-active cations and help differentiate between garnet types. It was found that different wavelength regions are sensitive to dif- ferent compositional and structural properties of garnets. Crystal-field absorptions involving Fe 2+ and/or Fe 3+ are responsible for the majority of spectral features in the garnet minerals examined here. There can also be spectral features associated with other cations and mechanisms, such as Fe 2+ –Fe 3+ and Fe 2+ –Ti 4+ intervalence charge transfers. The visible wavelength region is useful for identifying the presence of var- ious cations, in particular, Fe (and its oxidation state), Ti 4+ , Mn 2+ , and Cr 3+ . In the case of andradite, spessartine and uvarovite, the visible region absorption bands are characteristic of these garnets in the sense that they are associated with the major cation that distinguishes each: [6] Fe 3+ for andradite, [8] Mn 2+ for spessartine, and [6] Cr 3+ for uvarovite. For grossular, the presence of small amounts of Fe 3+ leads to ab- sorption bands near 0.370 and 0.435 μm. These bands are also seen in pyrope–almandine spectra, which also commonly have additional absorption bands, due to the presence of Fe 2+ . The common presence of Fe 2+ in the dodecahedral site of natural garnets gives rise to three Fe 2+ spin-allowed absorption bands in the 1.3, 1.7, and 2.3 μm regions, providing a strong spectral fingerprint for all Fe 2+ -bearing garnets studied here. Garnets containing Mn 2+ have additional visible (0.41 μm) spectral features due to [8] Mn 2+ . Gar- nets containing Cr 3+ , exhibits two strong absorption bands near 0.7 μm due to spin-forbidden [6] Cr 3+ transitions, as well as [6] Cr 3+ spin-allowed features near 0.4–0.41 μm and 0.56–0.62 μm, and [6] Cr 3+ spin- allowed transitions between 0.41 and 0.68 μm. Common silicate garnet spectra, in summary, are distinct from many other rock-forming silicates and can be spectrally distinct from one garnet species to another. Iron dominates the spectral properties of garnets, and the crystallographic site and oxidation state of the iron both affect garnet reflectance spectra. © 2017 Elsevier Inc. All rights reserved. 1. Introduction Garnets are a widely distributed group of rock-forming min- erals, and are important petrogenetic indicators. The presence of garnets is commonly indicative of high-pressure formation con- * Corresponding author at: Institute for Planetary Materials, Okayama University— Misasa, 827 Yamada, Misasa, Tottori, Japan. E-mail addresses: matthew.izawa@gmail.com, matthew_izawa@okayama-u.ac.jp (M.R.M. Izawa), e.cloutis@uwinnipeg.ca (E.A. Cloutis), stan.mertzman@fandm.edu (S.A. Mertzman), poitras-j@webmail.uwinnipeg.ca (J. Poitras). ditions (Juhin et al., 2010), though some garnets, especially cal- cic varieties, also form at lower pressures e.g., in skarn deposits (e.g., Meinert, 1992). Their crystal chemistry can provide informa- tion concerning the composition and petrogenetic conditions of their source region (e.g., Ghent, 1976; Holdaway, 2001). In addition to high pressure environments, garnets may also form during the crystallization of magma in some pegmatites and aluminous felsic intrusive rocks, by regional or contact metamorphism, and in hy- drothermal systems (Galoisy, 2013). The crystal structure of garnets allows for a wide range of chemical substitutions, some of which https://doi.org/10.1016/j.icarus.2017.09.005 0019-1035/© 2017 Elsevier Inc. All rights reserved.