Vol.:(0123456789) 1 3
Journal of Material Cycles and Waste Management
https://doi.org/10.1007/s10163-023-01842-1
REVIEW
Treatment and recycling of spent lithium‑based batteries: a review
Sameer Al‑Asheh
1
· Ahmad Aidan
1
· Teeba Allawi
1
· Fatma Hammoud
1
· Humaid Al Ali
1
· Maha Al Khamiri
1
Received: 15 January 2023 / Accepted: 24 October 2023
© The Author(s) 2023
Abstract
Lithium-ion batteries (LIBs) have a wide range of applications from electronic products to electric mobility and space explo-
ration rovers. This results in an increase in the demand for LIBs, driven primarily by the growth in the number of electric
vehicles (EVs). This growing demand will eventually lead to large amounts of waste LIBs dumped into landflls which can
cause serious environmental problems. To reduce this environmental impact, the need for efcient recycling technology
emerges. Furthermore, it has been proven that recycling waste LIBs consume less material and energy than producing new
ones from virgin materials. Therefore, this paper aims to review diferent recycling technologies including hydrometallurgy,
pyrometallurgy, direct recycling, and precise separation. The review concludes that hydrometallurgy might be the most
efcient method of recycling waste LIBs on an industrial scale.
Keywords LIB · Recycling · Hydrometallurgy · Pyrometallurgy · Precise separation
Abbreviations
ANVIL Adhesion Neutralization via Incineration
and Impact Liberation
CAM Cathode active material
CTR Carbothermic reduction
Cyanex 272 Bis(2,4,4-trimethyl-pentyl) phosphinic acid
D2EHPA Di(2-ethylhexyl) phosphoric acid
DEC Diethyl carbonate
DMC Dimethyl carbonate
EC Ethylene carbonate
ECS Eddy current separator
EMC Ethyl methyl carbonate
EV Electric vehicle
GHG Greenhouse gas
HTMR High-temperature melting recovery
LCO Lithium cobalt oxide
LFP Lithium iron phosphate
LIB Lithium-ion battery
LMO Lithium manganese oxide
NCA Nickel cobalt aluminum
NMC Nickel manganese cobalt
NMP N-methylpyrrolidone
PC Propylene carbonate
PTFE Polytetrafuoroethylene
PVDF Polyvinylidene fuoride
SEI Solid electrolyte interface
STF Single tube furnace
TBP Tributyl phosphate
TFA Trifuoroacetate
UHT Ultra-high-temperature smelting technology
Introduction
Recently, the demand for lithium-based battery-operated
electronics, solar panels, e-scooters and, most importantly,
electric vehicles (EVs), has increased. As a result, lithium-
ion batteries (LIBs) are being consumed at an exponential
rate and are becoming a necessary raw material for many
industries. If used batteries are not treated properly, they
will create a massive amount of environmental waste which
would be difcult to handle. This has been the interest of
environmentalists who have investigated diferent methods
to recycle such LIBs and, thus, reduce their damage to the
environment. Despite the diferent uses of LIBs, EVs have
the most prominent demand because their carbon footprint
over their entire lifetime is far less impactful on the envi-
ronment than that of an engine-driven car. Additionally,
unstable oil prices, relatively low maintenance costs and
better performance are other factors that contributed to the
* Sameer Al-Asheh
sslasheh@aus.edu
1
Department of Chemical and Biological Engineering,
College of Engineering, American University of Sharjah,
Sharjah, UAE