DOI: 10.1002/ijch.202000023
100 Years of Macromolecular Science
N. Gabriel Lemcoff,*
[a]
Charles E. Diesendruck,*
[b]
and Ehud Keinan*
[b]
The year 2020 is very special for polymer science. One
hundred years ago, Staudinger, considered by many the father
of polymer chemistry, published his famous manuscript “Über
Polymerisation”, describing several polymerization reactions
such as the polycondensation of dicrotonic esters, as well as
the polymerization of formaldehyde and styrene.
[1]
In 1922, he
coined the term “macromolecules”, which we still use to this
day to describe covalent polymers.
[2]
However, back in those
days, polymers, as described by Berzelius, had a completely
different meaning;
[3]
therefore, Staudinger’s work was not very
well received by the chemical community, to say the least.
[4]
Indeed, Staudinger had to embark on a personal crusade in
order to gain support for his concept of covalent macro-
molecules, as chemists at the time did not accept that
molecules above 5 kDa could be made. Staudinger’s pioneer-
ing work was eventually recognized when he received the
1953 Nobel Prize in chemistry “for his discoveries in the field
of macromolecular chemistry”. Therefore, following our
previous issues of Rosarium Philosophorum on Physical
Organic Chemistry, Structural Chemistry, Organic Synthesis
and Chemical Biology, this year, the Israel Journal of
Chemistry opens with a new Rosarium Philosophorum on
Macromolecular Chemistry, in which leaders in the field
describe key historical contributions, their own contributions
and personal views, as well as their perspectives on the future
of polymer science. The result is a marvelous compilation that
can serve as a guide for young (and less young) chemists
looking to contribute to this important and impactful aspect of
chemistry. It is also a short history lesson for those just curious
to learn more about the beautiful chemistry started by
Staudinger.
We have collected several important points from the
various contributions to this Rosarium:
Luscombe, Russel et al. describe the view of the IUPAC
Polymer Division concerning the role of polymers in society,
starting from the time preceding Staudinger, but highlighting
the important role Staudinger’s vision played in defining
macromolecules. These ideas allowed for the development of
new materials without which our lives would be significantly
more difficult. The history of polymers and macromolecules
within the annals of IUPAC is also summarized. Referring to
the role of polymers and polymer science in society, they
mention both the positive aspects and the current challenges,
especially those related to environmental impact. They also
forecast some of the expected advances in polymer science for
the next 30 years.
Baris Kiskan and Yusuf Yagci take us back in history to
Leo H. Baekeland and Bakelite, one of the most important
polymeric materials ever invented. The invention of the first
synthetic thermoset polymer paved the way for the develop-
ment of phenolic resins. As a curiosity, their account includes
the cover of Time magazine from 1924 featuring Baekeland,
one of the few practicing chemists to have gained this
distinction. Kiskan and Yagci explain the importance of the
synthesis conditions to the properties of phenolic resins,
including the ratio of phenol to formaldehyde, the catalyst
system and the reaction temperature and pH. They detail the
effects and types of curing methodologies and review some of
the chemical modifications typically used to enhance material
properties, such as long term thermo-oxidative stability, high
modulus or high char yields. A particularly interesting resin is
obtained when bisoxazolines are used as additional cross-
linking agents, affording materials with properties suitable
even for the aerospace industry. The account highlights the use
of renewable sources as starting materials and the emergence
of polybenzoxazines as competitors to the more established
Novolak resins. The authors conclude that phenolic resins and
their applications will continue to develop and expand during
their second century of existence.
Takuzo Aida and Bert E. W. Meijer describe the full
circle achieved with the amazing results obtained in the field
of supramolecular polymers. This is a very interesting story,
given that during Staudinger’s time, polymers, rubbers etc.
were considered non-covalent aggregates of small molecules
showing colloidal behavior. With the acceptance of Stau-
dinger’s concept of macromolecules, non-covalent interac-
tions, which play an enormous role in the structure and
[a] N. G. Lemcoff
Department of Chemistry, Ben-Gurion University of the Negev
P.O. Box 653, Beer-Sheva 84105, Israel
Phone: + 972-8-6461196
E-mail: lemcoff@bgu.ac.il
[b] C. E. Diesendruck, E. Keinan
The Schulich Faculty of Chemistry Technion-Israel Institute of
Technology, Technion City, Haifa, 32000, Israel
phone: + 972-4-8293664
E-mail: charles@technion.ac.il
keinan@technion.ac.il
Editorial
Isr. J. Chem. 2020, 60, 6 – 8 © 2020 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim 6