Int. J. Surface Science and Engineering, Vol. 11, No. 2, 2017 133
Copyright © 2017 Inderscience Enterprises Ltd.
The characterisation of surface treated silica-filled
and non-filled polydimethylsiloxane films
Michael J. Joyce*, Paul D. Fleming III and
Alexandra Pekarovicova
Department of Chemical and Paper Engineering,
Western Michigan University, USA
Email: mjoyce@wmich.edu
Email: dan.fleming@wmich.edu
Email: a.pekarovicova@wmich.edu
*Corresponding author
Abstract: In this work, various methods to enable tailoring of
polydimethylsiloxane film surfaces are implemented and compared to
determine their influence on surface energy and roughness. Films
were prepared containing various levels of hydrophilic silica filler.
Ultraviolet-ozone, and Piranha solution treatments were also implemented and
characterised. Lastly, the combination of both silica filler and treatments were
utilised and characterised to understand interactive effects. Influence of filler
loading, and surface treatment on roughness, and surface energy of films was
determined. Regardless of surface treatment, addition of silica significantly
influences total surface energy. Addition of silica influenced total surface
energy of the films by itself, and in combination with the Piranha and
UV-ozone treatments. The lowest surface energy was that of the control
Polydimethylsiloxane film 21.5 N/m. The overall highest surface energy
achieved was that of the 10% filled 30-minute Piranha solution treated sample,
having a surface energy of 44.1 N/m.
Keywords: polydimethylsiloxane; PDMS; surface treatments; UV-ozone;
Piranha solution; surface energy; medical devices; wettability; silica-fill;
ANOVA; biocompatible.
Reference to this paper should be made as follows: Joyce, M.J.,
Fleming III, P.D. and Pekarovicova, A. (2017) ‘The characterisation of surface
treated silica-filled and non-filled polydimethylsiloxane films’, Int. J. Surface
Science and Engineering, Vol. 11, No. 2, pp.133–147.
Biographical notes: Michael J. Joyce received his BS in Psychology and MS
in Paper and Printing Science from Western Michigan University, Kalamazoo
MI in 2012 and 2014, respectively. He is currently working as a Teaching
Assistant in the Department of Chemical and Paper Engineering while seeking
his PhD in Paper and Printing Sciences. He has worked on various
client-supported projects for industrial clients through the Center for the
Advancement of Printed Electronics and Center for Ink and Printability. He has
also served as a Teaching Assistant for courses regarding digital printing
processes, ink and colour production, and digital graphics. He has performed
projects utilising screen, flexo, gravure and inkjet print methods and has
created a novel processing method, enabling the creation of stand-alone printed
sensors. His doctoral work is focused on the study of metallic ink interactions
with PDMS substrates for creation of biocompatible sensors utilising various
printing processes.