Vol.:(0123456789) 1 3
Journal of Food Measurement and Characterization
https://doi.org/10.1007/s11694-020-00713-9
ORIGINAL PAPER
Determination of phenolics, organic acids, minerals and volatile
compounds of jujube (Ziziphus jujuba miller) jam produced
by under vacuum evaporation compared with open pan method
Alper Kuşçu
1
· Özcan Bulantekin
1
Received: 22 June 2020 / Accepted: 17 October 2020
© Springer Science+Business Media, LLC, part of Springer Nature 2020
Abstract
The jujube fruit (Ziziphus jujuba Miller) is used in alternative medicine due to its important bioactive components and is
well-suited for jam processing due to its high sugar content. In this study, changes in the chemical and aroma compounds
of jujube jams produced using the open-pan (OPJ) and vacuum evaporation (VEJ) methods were determined immediately
after production and after a storage period of 4 months. Concentrations of 5-hydroxymethylfurfural (HMF) in the OPJ and
VEJ were 13.94 and 1.53 mg/kg initially and 22.63 and 1.66 mg/kg after storage, respectively. Epicatechin was identifed
as the major phenolic component in jujube fruit and jams. Concentrations of phenolic compounds were higher in the VEJ
both before and after storage. It was determined that jujube jam is a good source of the minerals Fe, Ca, Zn, Se, and Cu.
Ascorbic acid loss was 86.47% in the OPJ versus 73.32% in the VEJ after production and continued during storage in both
jams. Numerous novel aroma compounds that are not found in fresh jujube fruit were produced as a result of the diferent
jam production methods. Signifcant advantages of the vacuum evaporation process have been determined in the production
of jujube jam compared to the open pan process.
Keywords Jujube jam · Vacuum evaporation · HMF · Organic acids · Phenolic compounds · Aroma compounds
Introduction
The jujube (Ziziphus jujuba Miller) is a unique fruit of
the Rhamnaceae family that has been used by people for
over 4000 years. Its natural distribution extends from Asia
(Afghanistan, China, India, Iran, Pakistan, Turkey, South
Korea, etc.) to Europe (Greece, Italy, Russia, Spain, etc.)
and the Australian continent [1, 2].
The jujube fruit is a good source of minerals, proteins,
sugars, organic acids, vitamin C, phenolics, and polysac-
charides. It also contains various bioactive compounds that
imbue the fruit with high nutritional value, functional prop-
erties, and health benefts [3, 4]. In traditional Chinese medi-
cine, the pharmaceutical efects of jujube fruit are utilized in
the treatment of diabetes, jaundice, diarrhea, urinary prob-
lems, ulcers, constipation, chronic bronchitis, liver disease,
wounds, depression, and insomnia. Previous studies have
shown that the bioactive components in jujube have anti-
proliferative, anti-infammatory, antioxidant, antiobesity and
antitumor efects and were protective against cardiovascular
diseases and type 2 diabetes [1, 5, 6]. Jujube fruit is pro-
cessed via numerous methods for consumption in various
forms, as a dried snack, sweetened tea syrup or teabags,
paste, soup, compote, pickle, jam, and wine.
Fruits and vegetables are preserved through various
methods. One of these methods is processing fruits and
vegetables into jam by concentrating and adding sugar.
Jams are popular food products due to their low cost, year-
round accessibility, and organoleptic properties. The con-
sumption of commercial jams has become increasingly
popular due to consumers’ modern lifestyles. Although
modern technologies are used today in commercial jam
production, they are still produced using home-cooking
methods [7]. In homemade jam production, fruit and sugar
are mixed at a certain ratio and the mixture is concentrated
at high temperatures to reach the fnal total soluble solid
* Alper Kuşçu
alperkuscu@sdu.edu.tr
Özcan Bulantekin
obulantekin@gmail.com
1
Engineering Faculty Department of Food Engineering,
Süleyman Demirel University, Isparta, Turkey