Distribution Statement A: Approved for public release; distribution is unlimited.
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American Institute of Aeronautics and Astronautics
Development of Composite Solid Propellants Based on
Dicyclopentadiene Binder
Stephen Bluestone
1
, Stephen D. Heister
2
, and Steven F. Son
3
Purdue University, West Lafayette, IN 47906
Benjamin L. Austin, Jr.
4
IN Space LLC, West Lafayette, IN 47906
Composite solid propellants have been formulated using polymerized dicyclopentadiene (DCPD) as a
binder. When the DCPD monomer is polymerized it produces an extremely tough plastic with excellent
tensile strength and fracture toughness. Studies were conducted with solids loadings in the 80-85% range
and a number of plasticizers are evaluated for improvement of ultimate strain capability. When compared to
the industry standard, hydroxyl-terminated polybutadiene (HTPB), it was found that DCPD composite
propellant had nearly 1.5 times the stress capacity while still exhibiting over 77% of the strain capacity of
HTPB-based composite propellant. The aluminized DCPD-based composite propellant also exhibits a
burning rate nearly twice that of HTPB. These factors combine make dicyclopentadiene-based composite
propellant a potentially attractive alternative for a number of missions demanding composite solid
propellants.
Nomenclature
a St. Robert’s Law pre-factor constant
AP ammonium perchlorate
CTPB carboxyl-terminated polybutadiene
DCPD Dicyclopentadiene
DPM Dual Planetary Mixer
HTPB hydroxyl-terminated polybutadiene
JATO Jet Assisted Take Off
LVDT Linear Variable Differential Transformer
n St. Robert’s Law power constant
P pressure (psi)
PBAN polybutadiene acrylonitirile
pDCPD poly-dicyclopentadiene
r burn rate (in/s)
ROMP Ring Opening Metathesis Polymerization
I. Introduction
For many years the field of composite solid propellants has been dominated by reliable
binders such as hydroxyl-terminated polybutadiene (HTPB) and polybutadiene acrylonitrile
(PBAN). These binders owe their success in the industry to years of research and
experimentation beginning with John Parsons and his asphalt/potassium perchlorate JATO
rockets.
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Seizing the potential of composite propellants other researchers went on to experiment
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Graduate Student, School of Aeronautics & Astronautics, 701 West Stadium Avenue, AIAA Member
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Professor, School of Aeronautics & Astronautics, 701 West Stadium Avenue, AIAA Associate Fellow
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Associate Professor, School of Mechanical Engineering, 585 Purdue Mall, AIAA Member
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President, 3495 Kent Avenue Suite G100, AIAA Senior Member
46th AIAA/ASME/SAE/ASEE Joint Propulsion Conference & Exhibit
25 - 28 July 2010, Nashville, TN
AIAA 2010-6589
Copyright © 2010 by the American Institute of Aeronautics and Astronautics, Inc. All rights reserved.