Modelling the properties of one-step
pigment-dyed and finished polyester/cotton
fabrics using response surface methodology
Muhammad Awais Imran
a,
* and Tanveer Hussain
b
a
Department of Textile Science, Faculty of Engineering, Science, and Technology, Indus
University, Karachi, 75300, Pakistan
Email: awais.imran89@gmail.com
b
Dean Faculty of Engineering and Technology, National Textile University, Faisalabad,
37610, Pakistan
Received: 25 December 2014; Accepted: 23 May 2016
Dyeing of polyester/cotton blended fabrics with two different classes of dyes for polyester and cotton is a
lengthy and expensive procedure owing to different fibre contents that need different auxiliaries, pH, and
temperature conditions. The aim of this study was to investigate and model the properties of a combined
pigment dyeing and hand-building finishing system for polyester/cotton blended fabrics. The one-step
process was investigated using response surface methodology, taking concentrations of pigment, softener,
and hand-building finish as experimental variables. It was found that increase in hand-building finish helps to
improve colour fastness at higher pigment concentrations but results in deterioration in fabric tear strength.
However, the decrease in tear strength can be minimised by increasing the softener concentration. For a
15 g l
1
pigment concentration, optimum fabric tear strength, crease recovery angle, bending length, and
dry and wet rubbing fastness properties were obtained using 60 g l
1
of softener and 65 g l
1
of hand-
building finish. The prediction equations developed in this study can be used to determine the required
amounts of softener and hand-building finish to achieve commercially acceptable results at different pigment
concentrations.
Coloration
Technology
Society of Dyers and Colourists
Introduction
Polyester/cotton (P/C) blended fabrics are very popular in
apparel and home textiles, with a worldwide share of
around 58.45% [1,2]. The blending of cotton with polyester
is governed by economy, durability, physical properties,
colour, and physical appearance factors. A P/C blend has
the advantage of polyester’s tensile strength, abrasion
resistance, and dimensional stability and cotton’s ability
to absorb water, and provides wearing comfort [3]. The
processing of P/C fabric is a lengthy and expensive proce-
dure owing to the combination of the two different fibre
chemistries. Polyester is commonly based on polyethylene
terephthalate (PET), whereas cotton is primarily composed
of cellulose. Generally, P/C fabrics are dyed using a two-
bath two-step method, where chemical cost and process
time are major concerns [4]. Several developments have
been reported by researchers to shorten the dyeing process
[5–11]. These developments have not been fully commer-
cialised owing to the high cost of the suitable dyes and
critical technical factors in the appropriate application
methods.
In contrast to dyeing with dyes, pigment dyeing is an
alternative approach of one-step dyeing of P/C fabrics
because of ease in application and no washing-off require-
ment after the dyeing process [12]. The fastness properties
of pigment-dyed fabrics are comparable with those of fabric
dyed with disperse/reactive dyes [13]. The control of
migration, good rubbing fastness, and stable dispersion
are some of the major problems faced by the textile industry
in pigment dyeing. Pigment dyeing with an exhaust system
is unpopular because of the nagging unevenness problem
[14]. In many textile processing industries, it is more
popular for pastel and dye-for-print fabrics, because very
light shades are possible by the pad-dry-cure method on a
stenter machine without using an infrared (IR) predryer.
However, some industries use IR predryers for medium
shades to avoid migration problems.
Hand-building finishing involves the application of stiff-
ening agents (mainly starch, polyvinyl acetate, or acrylic
copolymers) on fabrics to get the desired stiff handle and to
increase the weight of the fabrics [15]. The combination of
dyeing and finishing processes in one step is a more
economical and ecological approach that has been explored
by many researchers [16–23].
In the present work, the one-step pigment dyeing and
hand-building finishing process on P/C fabric was investi-
gated using the pad-dry-cure method. The aim of this study
was to model the properties of the one-step pigment dyeing
and hand-building finishing process using response surface
methodology (RSM), which has not been reported earlier to
the best of our knowledge. RSM comprises a collection of
mathematical and statistical techniques for modelling the
relationship between different factors/parameters of a pro-
cess and its response variables. Quadratic models of the
form
Y ¼ b
0
þ b
1
x
1
þ b
2
x
2
þ b
11
x
2
1
þ b
22
x
2
2
þ b
12
x
1
x
2
þ e
represent the relationship between response variable and
process parameters, where Y is the response variable, x
1
and
x
2
are the process parameters, b is the regression coefficient,
and e is the estimated error. The central composition design
of experiment (CCD) is not only efficient and economical
because of the smaller number of experiments (e.g. 20
414 © 2016 The Authors. Coloration Technology © 2016 Society of Dyers and Colourists, Color. Technol., 132, 414–420
doi: 10.1111/cote.12230