Citation: Lanzetta, A.; Papirio, S.;
Oliva, A.; Cesaro, A.; Pucci, L.;
Capasso, E.M.; Esposito, G.; Pirozzi, F.
Ozonation Processes for Color
Removal from Urban and Leather
Tanning Wastewater. Water 2023, 15,
2362. https://doi.org/10.3390/
w15132362
Academic Editors: Elia
Judith Martínez Torres and
Silvia Fiore
Received: 16 May 2023
Revised: 16 June 2023
Accepted: 25 June 2023
Published: 27 June 2023
Copyright: © 2023 by the authors.
Licensee MDPI, Basel, Switzerland.
This article is an open access article
distributed under the terms and
conditions of the Creative Commons
Attribution (CC BY) license (https://
creativecommons.org/licenses/by/
4.0/).
water
Article
Ozonation Processes for Color Removal from Urban and
Leather Tanning Wastewater
Anna Lanzetta
1
, Stefano Papirio
1
, Armando Oliva
1
, Alessandra Cesaro
1,
* , Luca Pucci
2
,
Emanuele Mariano Capasso
2
, Giovanni Esposito
1
and Francesco Pirozzi
1
1
Department of Civil, Architectural and Environmental Engineering, University of Napoli Federico II,
Via Claudio 21, 80125 Napoli, Italy; anna.lanzetta@unina.it (A.L.); stefano.papirio@unina.it (S.P.);
armando.oliva@unina.it (A.O.); giovanni.esposito1@unina.it (G.E.); francesco.pirozzi@unina.it (F.P.)
2
Gori Spa, 80056 Ercolano, Italy; lpucci@goriacqua.com (L.P.); ecapasso@goriacqua.com (E.M.C.)
* Correspondence: alessandra.cesaro@unina.it
Abstract: The need to ensure adequate levels of both human and environmental health protection
calls for the identification of efficient wastewater treatment processes that target the removal of
conventional pollutants as well as emerging contaminants, including synthetic dyes. This study
explores the potential of ozone for use in the decolorization of both pretreated tannery wastewater
and urban wastewater effluents. Different ozone contact times (15, 30, and 45 min) were applied
to such wastewater samples at an uncontrolled (7.5–8.2) pH as well as at a pH adjusted to 10. The
highest color removal efficiencies (REs) (>90%) were obtained with urban wastewater after a 45 min
contact time and at pH 10. Under the same conditions, a COD RE from 31 to 51% was achieved. Even
without pH adjustment, color and COD REs ranging from 81 to 92% and 39 to 41%, respectively, were
obtained. A preliminary evaluation of the costs associated with the implementation of an ozonation
stage within the wastewater treatment plant (WWTP) generating the urban wastewater used here
was carried out. The energy cost of the ozone treatment would account for a 69% increase in the
total energy cost of the WWTP, suggesting the need to identify proper strategies to enhance the
cost-competitiveness of this technology.
Keywords: advanced oxidation processes; color removal; emerging contaminants; tannery wastewater;
ozone
1. Introduction
Significant population growth, urbanization, and the global water crisis have gener-
ated an increasing demand for freshwater worldwide. The proper treatment of wastewater
plays a crucial role in supporting and maintaining the quality of aquatic ecosystem resources
as well as human health. The main determinants of the quality of receiving freshwater
bodies are chemical compounds and particles in water, such as nutrients, heavy metals, and
micro-organisms, whose concentrations depend on several factors, such as the origin of the
treated wastewater [1]. However, the presence of emerging contaminants (ECs), mainly
organics, including endocrine disruptors, pesticides, pharmaceuticals, hormones, toxins,
and industrial-related synthetic dyes [2,3], may compromise the water quality due to the
complexity associated with their treatment [4,5].
Normally, wastewater treatment plants (WWTPs) are designed and operated to re-
move mainly ammonia, total suspended solids (TSS), and the chemical oxygen demand
(COD) and to produce final high-quality effluents to be discharged in accordance with the
legally established standards. However, conventional WWTP processes are poorly efficient
for the removal of ECs [5], these being highly persistent and requiring particular operating
or environmental conditions due to their physicochemical characteristics [5]. Although EC
removal efficiencies (REs) in the ranges of 20–50% and 30–70% have been reported dur-
ing primary and secondary treatments, respectively, in most cases, conventional WWTPs
Water 2023, 15, 2362. https://doi.org/10.3390/w15132362 https://www.mdpi.com/journal/water