1932-4510/14©2014IEEE SEPTEMBER 2014 | IEEE NANOTECHNOLOGY MAGAZINE | 29
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CIRCLE—©CAN STOCK PHOTO/KEVDRAWS
CHING-HSIANG CHEN, WEI-NIEN SU, SUNNY HY, CHUN-JERN PAN, MEN-CHE TSAI, JOHN RICK, AND BING-JOE HWANG
Raman Scattering Surface
Signal Enhancement
SURFACE-ENHANCED RAMAN
scattering (SERS) is a powerful technique
that has been widely applied in differ-
ent fields to identify molecular structures
and characterize atomic interactions. In
this article, we introduce the theory and
instrumentation relevant to SERS induced
by silicon dioxide (SiO
2
)-coated shell iso-
lated gold nanoparticles (Au@SiO
2
) core–
shell nanoclusters (NCs) and nanorods
(NRs). We explain the synthetic meth-
ods used to generate Au@SiO
2
core–shell
NCs and NRs and show how they can
be manipulated for SERS applications,
including their use in biosensors that
are able to quantitatively analyze small
molecules and their roles in the struc-
tural identification of amorphous ultrathin
solid-state film materials and in elucidat-
ing the interphase reactions between the
electrode and electrolyte in lithium-ion
(Li-ion) batteries. Our findings support
the view that SERS techniques, used in
conjunction with metallic NCs or NRs,
can reduce the detection limits for tar-
get molecules and are, thus, applicable to
future studies of nanoscale materials.
INTRODUCTION TO RAMAN
SCATTERING TECHNOLOGY
Vibrational spectroscopy has been used
extensively in the chemical and materi-
als sciences to study gaseous, liquid, and
solid materials. This technique generally
provides more and better-resolved bands
containing more information than ultra-
violet and near-infrared electronic spec-
troscopy. Compared with electron energy
Digital Object Identifier 10.1109/MNANO.2014.2327252
Date of publication: 11 July 2014
Induced by Au@SiO
2
core-shell
nanoclusters and nanorods.