Structural order and clustering in annealed a -SiC and a -SiC:H
Cesar R. S. da Silva,
1
J. F. Justo,
2
and A. Fazzio
1
1
Instituto de Fı ´sica da Universidade de Sa ˜ o Paulo, CP 66318, CEP 05508-970, Sa ˜ o Paulo, SP, Brazil
2
Dep. Eng. Sistemas Eletroˆnicos, Escola Polite´cnica da Universidade de Sa ˜ o Paulo, CP 61548, CEP 05424-970, Sa ˜ o Paulo, SP, Brazil
~Received 14 August 2001; published 28 February 2002!
We carried out a theoretical investigation of the structural properties of annealed a -SiC and a -SiC:H. The
calculations were performed using the free volume Monte Carlo method combined with interatomic potentials.
Our prototype nanoparticle contained as much as 85 000 atoms which allows for a superior statistical sampling
of the material. The results show that C atoms segregate, forming small clusters embedded in an extensive Si
network. Si atoms are mostly contained in a single extensive network and a few small clusters. Unprecedented
detailed ring statistics analysis shows that C clusters do not form strictly C rings and that the introduction of
H increases the occurrence of microvoids in the structure. Moreover, the incorporation of H slightly reduces the
chemical order in the material and, to a larger extent, reduces the midrange structural order. Hydrogen also
relaxes bonding stress around atoms in the network. The results are consistent with the available experimental
data.
DOI: 10.1103/PhysRevB.65.104108 PACS number~s!: 61.43.Bn, 61.43.Dq
I. INTRODUCTION
Due to its electronic properties, amorphous silicon carbide
( a -SiC) has potential applications to optoelectronic
devices.
1
As a result, considerable effort has been devoted
over the last decade in order to refine the experimental tech-
niques and obtain SiC with the most desirable optical prop-
erties. However, to achieve that, several fundamental ques-
tions concerning the structural properties of SiC still need to
be addressed. For example, experimental results provide con-
troversial interpretations of the degree of chemical order
2,3
and of the role of hydrogen in the ordering of the alloy.
Amorphous silicon carbide films are usually grown by
plasma-enhanced chemical vapor deposition, from a mixture
of silane ~SiH
4
) and methane ~CH
4
) or other hydrocarbons.
Subsequent thermal annealing of these films leads to a large
increase in their photoluminescence, suggesting that relevant
structural changes occur under annealing.
4
Most of these
changes are the result of processes at the atomistic level and,
consequently, of chemical rebinding. It is therefore important
to understand the microscopic properties of a -SiC in order to
eventually improve its photoluminescence properties. In that
context, atomistic simulations can be a useful tool in inves-
tigating the structural properties of the material.
Atomistic simulation of the growth of a massive sample is
a formidable task in terms of computational resources. For-
tunately, a substantial amount of information can still be ob-
tained by studying the amorphous material generated by a
fast quench from the melt. Using this approach, amorphiza-
tion of semiconductors by laser ablation has already been
investigated.
5–9
Here, we report atomistic simulations of the
structural properties of unhydrogenated and hydrogenated
amorphous silicon carbide. Our investigations were carried
out by combining Monte Carlo ~MC! methods with inter-
atomic potentials in a simulated annealing procedure. Our
simulation system comprised as much as 85 000 atoms,
which allowed for a proper statistical sampling of the prop-
erties of SiC. By analyzing the ring and cluster statistics, to
investigate the medium-range order, we observe that carbon
atoms form small clusters, while silicon form large networks.
We also find that hydrogen changes the chemical order and
midrange structural order in the material.
II. METHODOLOGY
Atomistic simulations on the properties of amorphous sili-
con carbide have been performed using several levels of ap-
proximation, from ab initio
10
to empirical methods.
11,12
However, ab initio or even empirical methods still cannot
afford simulation cells comprising more than a hundred or a
few thousand atoms, respectively. Therefore, they do not
provide a relevant statistical sampling of the material, and
important questions could not be properly addressed. Re-
cently, an efficient algorithm, based on a free volume Monte
Carlo approach, has been developed
9
to study structural
properties of a -Si. In order to describe the interatomic inter-
actions, we used the Tersoff empirical potential.
13–15
This
potential has already been shown to provide a good descrip-
tion of several structural properties of silicon carbide.
12
Us-
ing that algorithm, we generated amorphous silicon carbide
from a molten material, which is slowly cooled down in a
simulated annealing procedure.
The prototype system is a cube with 32 000 Si and 32 000
C atoms in a zinc-blende structure organized as an array of
(20320320) unit cells, oriented in ^ 100& directions. The
simulation started with the system at a very high tempera-
ture, above the melting point. Consequently, the system
could lose any structural memory from the crystalline phase
after annealing. In simulating hydrogenated SiC, we added
21 000 hydrogen atoms in random positions after complete
melting of the system, followed by a subsequent annealing.
We emphasize that during annealing a small amount of H
was released on the surface of the system, but the total
amount of hydrogen inside the system was kept at around
20% atomic concentration. Both systems ( a -SiC and
a -SiC:H) were slowly quenched down to 10 K, when the
statistical analysis were performed.
Our simulations were carried out using open volume, so
PHYSICAL REVIEW B, VOLUME 65, 104108
0163-1829/2002/65~10!/104108~5!/$20.00 ©2002 The American Physical Society 65 104108-1