Iran Polym J
DOI 10.1007/s13726-016-0496-7
1 3
ORIGINAL PAPER
Manufacturing and structural analysis of antimicrobial kefiran/
polyethylene oxide nanofibers for food packaging
Anahita Jenab
1
· Rasoul Roghanian
1
· Giti Emtiazi
1
· Kamran Ghaedi
1
Received: 16 May 2016 / Accepted: 5 December 2016
© Iran Polymer and Petrochemical Institute 2016
Keywords Kefiran · ATR-FTIR · Electrospun nanofiber ·
Antimicrobial activity · Food packaging
Introduction
In electrospinning, electrostatic forces is used to produce
polymeric, ceramic and composite continuous ultrafine fib-
ers with diameters ranging from microns to few nanom-
eters. This technique is versatile, simple and convenient
[1]. Using this method, many kinds of nanofibers from
polymers, e.g., polyethylene oxide (PEO), polyacrylonitrile
(PAN) and polyvinyl alcohol (PVA), have been made with
optoelectronic properties.
Electrospun nanofibers can simulate the nanofibrous
structure of the native extracellular matrix. Moreover, the
scaffolds produced by electrospinning offer a high sur-
face area to volume ratio, high length/diameter ratio which
would improve mechanical performance and flexibility in
surface functionalities. There has been much interest in
extending this technique to prepare uniform fibers with
novel compositions and morphologies for several applica-
tions [2].
In recent years, increasing demand for natural polymers
in several applications has led to interest in exopolysaccha-
rides of microorganisms [3, 4]. Some of the microbial poly-
saccharide characteristics are biological degradation, bio-
compatibility, cost-effectiveness, availability, and similarity
to extracellular matrix, their capability of inherent cellular
reaction and connectivity to cells [5]. They are applied in
food, pharmaceutical, and chemical industries as biofloccu-
lants, bioabsorbents, heavy metal removal agents, and drug
delivery agents.
Lactic acid bacteria that excrete polysaccharide with
high molecular weight have been extensively studied in
Abstract Kefiran, a branched glucogalactan, is a useful
microbial polysaccharide produced by lactic acid bacte-
ria. The aim of this study was to evaluate the antimicrobial
activity of kefiran nanofibers as a biocontrol agent for food
packaging as well as food preservation. Thus, kefiran/poly-
ethylene oxide (PEO) nanofibers were fabricated using the
electrospinning method. Kefiran was produced from raw
milk with 0.5% fat and 10 g of kefir grain and was sepa-
rated from it by ethanol. Structural analysis of kefiran was
detected by means of nuclear magnetic resonance and Fou-
rier transforms infrared spectroscopy (FTIR). Antimicro-
bial properties of kefiran were assayed against Rhizoctonia,
Pseudomonas sp. (isolated from soil at Isfahan Univer-
sity) and Staphylococcus aureus (S. aureus). Electrospun
kefiran/PEO nanofibers were characterized by scanning
electron microscopy, optical microscopy and ATR-FTIR
techniques. Hydrophilicity and in vitro biodegradation
of the kefiran/PEO nanofibers were investigated, as well.
The results showed that the mean diameter of the nanofib-
ers was 607.5 nm. The contact angle measurement result
was 51.5° ± 0.71 with normal hydrophilicity. First of all,
antimicrobial properties of kefiran were confirmed against
different types of microorganisms. Moreover, the result
obtained in this study showed that kefiran/PEO nanofibers
with oxidizing functional groups on them have antimicro-
bial activity against S. aureus. Biodegradation of kefiran/
PEO nanofibers was also confirmed by FTIR.
* Rasoul Roghanian
r.roghanian@sci.ui.ac.ir
1
Department of Biology, Faculty of Science, University
of Isfahan, Isfahan, Iran