Iran Polym J (2016) 25:89–109
DOI 10.1007/s13726-015-0405-5
1 3
REVIEW
A state‑of‑the‑art review on the mathematical modeling
and computer simulation of rubber vulcanization process
Mir Hamid Reza Ghoreishy
1
Received: 14 March 2015 / Accepted: 14 June 2015 / Published online: 15 December 2015
© Iran Polymer and Petrochemical Institute 2015
Introduction
Curing or vulcanization process is a fundamental step dur-
ing the manufacturing of rubber articles, especially tires
and other high thickness products. It plays an important
role in achieving accurate and low tolerance shape and
also pre-designed physical and mechanical properties of
the final product. Therefore, optimum determination of
time arrangements and temperature variations during heat-
ing and cooling or post-cure steps is of prime importance.
Moreover, due to high energy consumption of this stage,
optimization also leads to more economical process. How-
ever, owing to the low thermal diffusivity in rubbers and
also applying time-varying operating conditions, the tem-
perature field inside the article is not only non-uniform but
also changes with time. Therefore, difficulties arise when a
simple cure evaluation curve, generally obtained by a disk
rheometer at constant temperature, is intended to be used
to predict the time and temperature required for the com-
pleteness of a curing process. Traditionally, a full experi-
mental method is adopted in which the thermal history at
various points inside the article (especially high thickness
zones) is measured. The measured temperature can be
converted to state of cure or degree of cure by the use of
a kinetics equation, and thus, the time required to achieve
a complete cycle is determined. Obviously, this method is
time-consuming and expensive since for every experiment
at least a rubber article should be damaged. Alternatively,
determination of the thermal history and its variation inside
a product by solving heat transfer equation using an appro-
priate numerical method in conjunction with a computer
code are the preferred methods in today’s rubber industry.
Recently, we have briefly reviewed the numerical simula-
tion of the curing process of rubber articles [1] and pre-
sented some practical techniques to predict the temperature
Abstract This monograph reviews and examines the
theoretical background and literature published so far for
the mathematical modeling and simulation of the rubber
vulcanization process. This work has been organized in
the following way. First, an introductory section is given,
which provides a brief overview of the topic and the aim
and scope of the paper. Then, it goes on to give a compre-
hensive overview of the historical background up to present
state. It is tried here not only to consider rubber vulcani-
zation process, but the curing of other thermoset polymers
are examined. The third section presents the mathematical
modeling of the curing process and focuses on four key
items including heat transfer governing equations, thermal
properties of rubbers and their measurements, kinetics of
the curing reaction and solution methodology. In this part,
the details of the solution methods for the governing equa-
tions and also different types of kinetics of curing reac-
tions are studied. The fourth section presents the findings
of some research works carried out in this field, which is
divided into two subsections as tires and non-tires applica-
tions. A brief summary on the presented work and some
suggestions for future research are introduced in the fifth
section, and finally the bibliography of this review is given.
Keywords Rubber · Vulcanization · Simulation · Finite
element method · Kinetics · Tire
* Mir Hamid Reza Ghoreishy
m.h.r.ghoreishy@ippi.ac.ir
1
Department of Rubber Processing and Engineering, Faculty
of Processing, Iran Polymer and Petrochemical Institute,
Tehran, P.O. Box 14975-112, Iran