Chemico-Biological Interactions 115 (1998) 85 – 107 Protection of DNA in HL-60 cells from damage generated by hydroxyl radicals produced by reaction of H 2 O 2 with cell iron by zinc-metallothionein Wael G. Elgohary, Sarfraz Sidhu, Susan O. Krezoski, David H. Petering, Robert W. Byrnes * Department of Chemistry, P.O. Box 413, Uni6ersity of Wisconsin -Milwaukee, Milwaukee, WI 53201, USA Received 20 February 1998; received in revised form 26 May 1998; accepted 11 June 1998 Abstract Scavenging of hydroxyl radicals ( OH) by the zinc form of metallothionein (ZnMT) was studied in HL-60 cells and in nuclei from such cells previously treated with ZnCl 2 (ZnMT cells). Cells were grown for 48 h to label DNA for alkaline elusion experiments. During the last 24 h 0.1 mM ZnMT was included to induce ZnMT. Generation of DNA single-strand breaks (SSBs) by H 2 O 2 in cells (5 ×10 5 /ml) treated at 4° was increased by approximately 70% in Zn-treated cells by comparison with control cells. These cells had grown from an initial concentration of 5 ×10 5 /ml to a concentration at harvest of 16 ×10 5 /ml. Cells started at 6 ×10 5 /ml and growing to a final concentration of 20 ×10 5 /ml did not exhibit a similar increase in SSBs. This elevation in SSBs was traced to an increase in cell Fe content which exhibited a sharp dependence upon concentrations of cells and of ZnCl 2 at the time of addition. The diffusion distance (d ) from Fe to DNA of ZnMT cells treated with H 2 O 2 was found to be 3.4 nm. This compares with a distance of 6.1 nm in control cells. SSB generation by hydroxyl radicals formed by 137 Cs-g rays in Zn-treated cells decreased by 12%, accompa- Abbre6iations: DMSO, dimethyl sulfoxide; DRF, dose reduction factor; NEB, nuclear extraction buffer; NEM, N-ethylmaleimide; NTB, nuclear treatment buffer; MT, metallothionein; SSB, single strand break. * Corresponding author. Present address: 3950 Mahaila Avenue, Apt. J-15, San Diego, CA 92122, USA. Tel: +1 619 6239756 0009-2797/98/$ - see front matter © 1998 Elsevier Science Ireland Ltd. All rights reserved. PII S0009-2797(98)00061-1