Often the performance of a material is governed by
how its surface interacts with its environment, and
this frequently depends upon the structure and
composition of that surface at the molecular scale.
This basic fact has driven the development of surface
analytical instrumentation for decades. An ideal tool
would allow the researcher to know the surface
composition of their sample with molecular
resolution and in a realistic environment, and even to
monitor these molecular processes directly as the
sample interacts with its environment.
While the search for the perfect instrument is still
ongoing, in 1982 this effort was significantly enhanced by
the invention of the scanning tunneling microscope (STM),
allowing the direct spatial imaging of conductive surfaces
with atomic resolution under a wide range of environments.
This invention sparked the imagination of scientists and
engineers worldwide, and the ensuing years witnessed the
development of a regular alphabet soup of different
techniques that are broadly known as scanning probe
microscopy (SPM). Of these techniques, none is so pervasive
and broadly applicable as atomic force microscopy (AFM).
Briefly, AFM operates by placing a sharp tip in such close
proximity to a sample that their interaction can be measured.
Unlike traditional spectroscopic surface analytical
instruments, the high resolution afforded to AFM is offset by
the remarkably low data content, which is largely mechanical
and physical in nature with little chemical or compositional
information. Initial efforts to enhance the data content of
AFM focused on increasing the number of modes.
Atomic force microscopy (AFM) has revolutionized
surface characterization by allowing the researcher to
examine the molecular structure of virtually any
sample under virtually any environmental condition.
The AFM is used to produce information about
surface topography, elasticity, friction, adhesion,
charge density, magnetic structure, or even long-
range effects. Compared to traditional spectroscopic
surface analytical tools, the AFM suffers from a
remarkably low data content. Chemical modification
of the tip incorporates chemical information within
the measurements. In this way, researchers have
obtained compositional maps of heterogeneous
materials, measured single-molecule interaction
forces between biopolymers, and even differentiated
some nuances of cell membranes.
by John-Bruce D. Green, Ademola Idowu, and Sandra S. F. Chan
Modified tips:
molecules to cells
Department of Chemistry,
University of Alberta,
Edmonton, AB T6G 2G2
Canada
Email: john.green@ualberta.ca
ISSN:1369 7021 © Elsevier Science Ltd 2003 February 2003 22