S1
Supporting Information for
Domino Prins/Pinacol reaction for the stereoselective synthesis of
spiro[pyran-4,4'-quinoline]-2',3'-dione derivatives
B. V. Subba Reddy,
[a]*
S. Gopal Reddy,
[a,b]
M. Durga Prasad,
[a]
Manika Pal Bhadra
[b]
B. Sridhar
[c]
a
Natural Product Chemistry,
b
Centre for Chemical Biology,
c
Laboratory of X-ray Crystallography, CSIR-Indian
Institute of Chemical Technology, Hyderabad –500 007, India. E-mail:basireddy@iict.res.in.
OH
HO
DCM, 0
o
C
3 4
BF
3
.OEt
2
5
N
O
N
O
O
O
R
R-CHO
Table of Contents
1. General procedure..........................................................................S2-S4
2. Characterization data of 5(a-r) & 3...............................................S4-S12
3. Copies of
1
H &
13
C NMR spectra of 5(a-r) & 3..........................S13-S32
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry.
This journal is © The Royal Society of Chemistry 2015