American Journal of Cancer Prevention, 2015, Vol. 3, No. 2, 45-50
Available online at http://pubs.sciepub.com/ajcp/3/2/4
© Science and Education Publishing
DOI:10.12691/ajcp-3-2-4
Anti-proliferative, Cytotoxicity and Anti-oxidant
Activity of Juglans regia Extract
Tajamul Islam Shah
1,*
, Ekta Sharma
2
, Gowhar Ahmad Shah
3
1
Department of Research, Jawaharlal Nehru Cancer Hospital and Research Centre, Bhopal, India
2
Department of Botany, Benazeer College of science, Bhopal, India
3
Department of Zoology, Benazeer College of Science and Commerce Bhopal, India
*Corresponding author: taju.zoology@gmail.com
Received April 01, 2014; Revised April 09, 2014; Accepted April 20, 2015
Abstract Objective: Juglans regia (walnuts), the royal species from Junglandaceae family, well-known for its
valuable medicinal uses, their regular consumption may have beneficial effects against oxidative stress mediated
diseases including cancer. The present study was aimed to explore the total phenolic content, anti-proliferative and
anti-oxidant activity of Juglans regia leaves. Methods: The leaf powder was extracted using different solvents and
subjected for phytochemical investigation. The total phenolic contents were determined by the Folin–Ciocalteu
method. The extracts comprising a good amount of secondary metabolites especially polyphenols were used to
evaluate their antioxidant activity using Fenton’s reagent reaction and DPPH scavenging assay, while cytotoxic and
anti-proliferative activity against B16F10 mice melanoma and A375 human melanoma cell were screened using
MTT Assay. Observation: Methanolic extract presented the highest total phenolic content (94.39 ± 5.63 mg of
GAE/g of extract) as compared to aqueous extract (27.92 ± 1.40 mg of GAE/g of extract). Similarly, methanolic
extract presented the highest antioxidant activity (EC
50
of 0.250mg/ml) followed by water extract (EC
50
of
0.325mg/ml) in Fenton’s reaction and 0.199 ± 0.023 and 2.991 ± 0.740, respectively in DPPH assay. The extracts
showed concentration dependent growth inhibition activity (IC
50
0.234 and 0.304mg/ml) against B16F10 mice
melanoma and A375 human melanoma cell line (IC
50
0.298 and 0.350mg/ml) respectively. The extracts proved least
toxic when treated with normal lymphocytes. The results indicate that walnut leaves are an excellent source of
antioxidant and anti-cancerous agents and may prove fruitful herbal remedy in near future. However, the extracts
proved effective against mice melanoma and human melanoma cells. Despite, more study is required before coming
to any conclusion.
Keywords: J. regia, anti-oxidant, anti-proliferative, B16F10, A375, Lymphocytes, MTT
Cite This Article: Tajamul Islam Shah, Ekta Sharma, and Gowhar Ahmad Shah, “Anti-proliferative,
Cytotoxicity and Anti-oxidant Activity of Juglans regia Extract.” American Journal of Cancer Prevention, vol. 3,
no. 2 (2015): 45-50. doi: 10.12691/ajcp-3-2-4.
1. Introduction
Epidemiological studies have consistently shown that
there is a clear significant positive association between
regular consumption of fruits, nuts and vegetables, and a
reduced incidence of ischemic heart disease and some
types of cancer, particularly stomach, oesophagus, lung,
oral cavity and pharynx, endometrial, pancreas and colon
cancers [1,2,3,4,5]. These antioxidant and chemopreventive
properties have been attributed to their high content of
natural antioxidants, especially ascorbic acid (vitamin C),
tocopherols (vitamin E), b-carotene (provitamin A),
anthocyanins and other polyphenols [6,7,8,9]. Several
studies showed that phenolic compounds are the major
bioactive phytochemicals with human health benefits
[10,11,12]. In fact, many authors have reported a direct
relationship between total phenolic content and
antioxidant activity in numerous seeds, fruits and
vegetables [9,10,11,12,13].
The Juglans genus (family Juglandaceae) comprises
several species and is widely distributed throughout the
world. The walnut tree (Juglans regia L.) is its well-known
member, constituting an important species of deciduous
trees found primarily in temperate areas and cultivated
commercially throughout southern Europe, northern
Africa, eastern Asia, United States and western South
America. In Portugal, walnut trees can be found all over
the country, being the nuts very popular and largely
consumed as part of the Mediterranean diet. Nevertheless,
not only dry seeds (nuts) are used but also green walnuts,
shells, bark, green husks (epicarps) and leaves, which
have been used in the cosmetic and pharmaceutical
industries [14].
Walnut leaves are considered a source of healthcare
com- pounds, and have been widely used in traditional
medicine for treatment of skin inflammations,
hyperhidrosis and ulcers and for its antidiarrheic, anti-
helmintic, antiseptic and astringent prop- erties [15]. In
Portugal, as in some other European countries, especially
in rural areas, dry walnut leaves are fre- quently used to