Adv Polym Technol. 2017;1–13. wileyonlinelibrary.com/journal/adv | 1 © 2017 Wiley Periodicals, Inc.
Received: 18 March 2017
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Accepted: 19 July 2017
DOI: 10.1002/adv.21875
RESEARCH ARTICLE
Improvements in mechanical strength and thermal stability of
injection and compression molded components based on Poly
Lactic Acids
Clizia Aversa
1
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Massimiliano Barletta
2,1
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Annamaria Gisario
3
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Elisa Pizzi
1
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Michela Puopolo
1
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Silvia Vesco
1
1
Dipartimento di Ingegneria
dell’Impresa, Università degli Studi di
Roma Tor Vergata, Roma, Italy
2
Dipartimento di Ingegneria, Università
degli Studi Roma Tre, Roma, Italy
3
Dipartimento di Ingegneria Meccanica ed
Aerospaziale, Sapienza Università degli
Studi di Roma, Roma, Italy
Correspondence
Massimiliano Barletta, Dipartimento di
Ingegneria, Università degli Studi Roma
Tre, Roma, Italy.
Email: barletta@ing.uniroma2.it
Funding information
LIFE + Programme (2014-2020), Grant/
Award Number: LIFE-PLA4COFFEE ENV/
IT/000744; European Commission
Abstract
Degradable polymers are limited by their often-insufficient mechanical and thermal
properties, which limit their usage to single-use packaging items at room temperature
and in dry conditions. In this respect, the present work deals with the manufacture of
custom-built Poly Lactic Acids (PLAs), which are designed to be compostable, suit-
able for food contact and are characterized by a good compromise between mechani-
cal properties and thermal stability. A commercial grade PLA was, therefore,
compounded in a twin-screw co-rotating extruder by the use of specific additives:
maleated and glycidyl methacrylate PLAs as compatibilizers/chain extenders and
microlamellar talc as mineral filler/nucleation promoter. After pelletizing, the result-
ing compounds were melt-processed by injection and compression molding.
Differential scanning calorimetry, flexural tests in static machine and top-hat cylin-
drical flat indentations were performed to evaluate the thermal and mechanical
response of the molded components. The experimental findings show that crystalli-
zation of the PLA can be controlled by fine-tuning the compound formulation as well
as by properly setting the processing parameters. In addition, achievement of the
appropriate crystallization degree in the polymer can lead to molded components,
which exhibit improved mechanical strength and high thermal stability.
KEYWORDS
compostable polymer, mechanical response, melt processing, molding, thermal stability
1
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INTRODUCTION
In the wide range of polymeric materials from renewable
resources, the class of materials based on poly(lactic acid)
(PLA) is a very promising alternative for the replacement
of common plastics derived from petroleum, especially for
applications in the rigid and flexible packaging industry.
Although PLA is a biodegradable material with highly con-
trollable compostability, its thermal and mechanical prop-
erties make it hypothetically suitable for the production of
durable goods, such as structural parts in cross-application
(components and objects for the automotive, domestic, elec-
tronic fields). However, several limitations have restricted the
launch of a massive usage of PLA in industrial production,
mainly due to the high-production cost of the raw material.
In addition, the thermo-mechanical stability of PLA is not
yet comparable to traditional noncompostable plastics that
are extensively present on the market.
On one hand, PLA shows the tendency to behave as an
excessively rigid and/or brittle plastic, featuring too low
toughness properties. On the other hand, PLA shows a mol-
ten phase that is not thermally resistant during conventional