Optical Properties of Highly Transparent Polypropylene
Cast Films: Influence of Material Structure, Additives,
and Processing Conditions
Katharina Resch
Polymer Competence Center Leoben GmbH, Parkstrasse 11, 8700 Leoben, Austria
Gernot M. Wallner
Institute of Materials Science and Testing of Plastics, University of Leoben, Franz-Josef Strasse 18,
8700 Leoben, Austria
Christian Teichert
Institute of Physics, University of Leoben, Franz-Josef Strasse 18, 8700 Leoben, Austria
Gu¨ nther Maier
Material Center Leoben Forschung GmbH, Franz-Josef Strasse 13, 8700 Leoben, Austria
Markus Gahleitner
Borealis GmbH, St. Peter-Strasse 25, 4021 Linz, Austria
Polypropylene homopolymers and ethylene/pro-
pylene-random-copolymers formulated with and with-
out anti-blocking additives were extruded to cast films
with an industrial scale extruder equipped with a soft
box, a specific air knife that expels a higher volume of
air at lower velocity. The films were analyzed as to
their optical properties haze and clarity. A comprehen-
sive topographical characterization was performed
using atomic force microscopy (AFM) and confocal
microscopy. To obtain morphological information on a
nanometer scale AFM phase imaging, micro-thermal
analysis and small angle X-ray scattering (SAXS) were
done. A significant effect of additives and processing
conditions on the film topography and the optical
properties was revealed. The films without anti-block-
ing and antacid aids showed the best optical proper-
ties and lowest vertical roughness fluctuations. In
contrast, the addition of anti-blocking and antacid
aids reduced the optical properties associated with an
increase in surface roughness. While for films without
anti-blocking aids an enhanced soft box condition re-
sulted in lower vertical fluctuations of roughness and
better optical properties, the behavior was in reverse
for films with anti-blocking aid. By means of SAXS
crystalline lamellae with a thickness of about 2.5 nm
were detected. High-resolution phase imaging AFM
yielded thicker crystal lamellae on the film surface.
POLYM. ENG. SCI., 46:520 –531, 2006. © 2006 Society of Plas-
tics Engineers
INTRODUCTION
Polymer films used in the packaging industry often have
to fulfill high requirements as to their optical properties.
Particularly in medical applications, special optical proper-
ties such as low haze and high clarity are key issues.
Polypropylene (PP) cast films are in use for packaging of
drugs and medical substances. Because of technical and
economic reasons, such films should be produced in a
high-speed extrusion process.
The disturbances affecting the optical properties of melt-
processed films may be due to the structure of the bulk of
the polymer as well as to the structure of the film surface,
whereas the latter is predominant. Earlier studies [1– 4],
especially by Ashizawa et al. [2], Bheda and Spruiell [3],
and White et al. [4], who investigated various blown films
of semicrystalline and amorphous polymers, established the
surface as primary location of scattering by determining
excellent correlations between surface roughness and opti-
Correspondence to: Katharina Resch; e-mail: resch@pccl.at
DOI 10.1002/pen.20503
Published online in Wiley InterScience (www.interscience.wiley.
com).
© 2006 Society of Plastics Engineers
POLYMER ENGINEERING AND SCIENCE—2006