Indonesian Physical Review
Volume 07 Issue 02, May 2024
P-ISSN: 2615-1278, E-ISSN: 2614-7904
281
Synthesis and Characterization of Activated Carbon Prepared
from Rice Husk by Physics-Chemical Activation
Anak Agung Gde Suyoga Wiguna
1*
, Ida Bagus Putu Mardana
1*
, Putu Artawan
1*
1
Physics and Science Teaching Department, Faculty of Mathematics and Natural Science, Ganesha University of
Education, Indonesia
Corresponding Authors E-mail: anak.agung.gde@undiksha.ac.id, putu.mardana@undiksha.ac.id,
artawan.putu@undiksha.ac.id,
Article Info Abstract
Article info:
Received: 16-02-2024
Revised: 16-05-2024
Accepted: 22-05-2024
Keywords:
Synthesis;
characterization; activated
carbon; Rice husk
How To Cite:
A. A. G. S. Wiguna, I. B.
P. Mardana, P. Artawan,
“Synthesis and
characterization of rice
husk activated carbon by
HCl activation,”
Indonesian Physical
Review, vol. 7, no. 2, p
281-290, 2024.
DOI:
https://doi.org/10.29303/ip
r.v7i2.311
Activated carbon is an amorphous carbon material predominantly
composed of free carbon atoms with high adsorption capacity. The
amorphous structure in activated carbon affects its adsorption
capacity; the higher the percentage of amorphous carbon, the greater
the adsorption capacity of the activated carbon. Activated carbon can
be obtained from rice husk waste, which contains 30-40% C in
cellulose, hemicellulose, and lignin. Therefore, this study was
conducted to observe activated carbon's phases, morphology,
elemental composition, and particle size. Activated carbon was
synthesized using a physics-chemical activation method, which began
with washing the rice husk samples, followed by air drying,
carbonizing into charcoal, and grinding it finely. The rice husk
charcoal powder was then physically activated at a temperature of
500℃. The physically activated product was then chemically activated
using 6M HCl with a charcoal-to-activator ratio of 1:10 (m/V), stirred
at 250 rpm for 1 hour, and then allowed to settle for 24 hours. It was
then washed and dried to produce activated carbon powder. XRD test
results showed diffraction peaks at 2θ = 22.23° without sharp or
pointed peaks, indicating that the activated carbon has an amorphous
structure. SEM test results showed the morphology of rice husk-
activated carbon with spherical particle shapes and a particle size
distribution of 20-70 nm. EDX test results showed that the rice husk
activated carbon is predominantly composed of C, O, and Si with
respective percentages of 54.31%, 40.04%, and 2.49%.
Copyright © 2024 Authors. All rights reserved.
Introduction
One sector that plays a crucial role in Indonesia's economic growth is industry. The industrial
sector produces various products for human needs and exports. Adequate resources must
support the sustainability of the sector in Indonesia. One abundant resource in Indonesia is its
natural resources. Indonesia is an agricultural country where 40% of its population is involved
in farming. One of the leading agricultural products in Indonesia is rice. This is because rice is
a crucial commodity as a staple food for Indonesians. Based on data from the Central Statistics