Citation: Drioiche, A.; Baammi, S.;
Zibouh, K.; Al Kamaly, O.; Alnakhli,
A.M.; Remok, F.; Saidi, S.; Amaiach,
R.; El Makhoukhi, F.; Elomri, A.; et al.
A Study of the Synergistic Effects of
Essential Oils from Origanum compactum
and Origanum elongatum with
Commercial Antibiotics against Highly
Prioritized Multidrug-Resistant Bacteria
for the World Health Organization.
Metabolites 2024, 14, 210. https://
doi.org/10.3390/metabo14040210
Academic Editors: Luke E. K. Achenie
and Andres Fernando Gonzalez
Barrios
Received: 14 March 2024
Revised: 30 March 2024
Accepted: 2 April 2024
Published: 7 April 2024
Copyright: © 2024 by the authors.
Licensee MDPI, Basel, Switzerland.
This article is an open access article
distributed under the terms and
conditions of the Creative Commons
Attribution (CC BY) license (https://
creativecommons.org/licenses/by/
4.0/).
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Article
A Study of the Synergistic Effects of Essential Oils from
Origanum compactum and Origanum elongatum with
Commercial Antibiotics against Highly Prioritized
Multidrug-Resistant Bacteria for the World Health Organization
Aziz Drioiche
1,2,
* , Soukayna Baammi
3
, Khalid Zibouh
1
, Omkulthom Al Kamaly
4
, Anwar M. Alnakhli
4
,
Firdaous Remok
1
, Soukaina Saidi
1
, Rachid Amaiach
5
, Fadoua El Makhoukhi
1
, Abdelhakim Elomri
6
and Touriya Zair
1,
*
1
Research Team of Chemistry of Bioactive Molecules and the Environment, Laboratory of Innovative Materials
and Biotechnology of Natural Resources, Faculty of Sciences, Moulay Ismail University, B.P. 11201, Zitoune,
Meknes 50070, Morocco; k.zibouh@edu.umi.ac.ma (K.Z.); f.remok@edu.umi.ac.ma (F.R.);
soukaina.saidi@usms.ma (S.S.); elmakhoukhi@cnrst.ma (F.E.M.)
2
Medical Microbiology Laboratory, Mohamed V. Hospital, Meknes 50000, Morocco
3
Bioinformatics Laboratory, College of Computing, Mohammed VI Polytechnic University,
Ben Guerir 43150, Morocco; soukayna.baammi@um6p.ma
4
Department of Pharmaceutical Sciences, College of Pharmacy, Princess Nourah bint Abdulrahman University,
P.O. Box 84428, Riyadh 11671, Saudi Arabia; omalkmali@pnu.edu.sa (O.A.K.); amalnklee@pnu.edu.sa (A.M.A.)
5
Laboratory of Materials, Processes, Catalysis and Environment, School of Technology, University Sidi
Mohamed Ben Abdellah, Fez 30000, Morocco; rachid.amaiach@usmba.ac.ma
6
UNIROUEN, INSA Rouen, CNRS, COBRA (UMR 6014), Normandie University, 76000 Rouen, France;
hakim.elomri@univ-rouen.fr
* Correspondence: a.drioiche@edu.umi.ac.ma (A.D.); t.zair@umi.ac.ma (T.Z.); Tel.: +212-600394841 (A.D.)
Abstract: The irrational use of antibiotics has favored the emergence of resistant bacteria, posing
a serious threat to global health. To counteract antibiotic resistance, this research seeks to identify
novel antimicrobials derived from essential oils that operate through several mechanisms. It aims
to evaluate the quality and composition of essential oils from Origanum compactum and Origanum
elongatum; test their antimicrobial activity against various strains; explore their synergies with
commercial antibiotics; predict the efficacy, toxicity, and stability of compounds; and understand
their molecular interactions through docking and dynamic simulations. The essential oils were
extracted via hydrodistillation from the flowering tops of oregano in the Middle Atlas Mountains in
Morocco. Gas chromatography combined with mass spectrometry (GC-MS) was used to examine their
composition. Nine common antibiotics were chosen and tested alone or in combination with essential
oils to discover synergistic effects against clinically important and resistant bacterial strains. A
comprehensive in silico study was conducted, involving molecular docking and molecular dynamics
simulations (MD). O. elongatum oil includes borneol (8.58%), p-cymene (42.56%), thymol (28.43%), and
carvacrol (30.89%), whereas O. compactum oil is mostly composed of γ-terpinene (22.89%), p-cymene
(15.84%), thymol (10.21%), and (E)-caryophyllene (3.63%). With O. compactum proving to be the most
potent, these essential oils showed antibacterial action against both Gram-positive and Gram-negative
bacteria. Certain antibiotics, including ciprofloxacin, ceftriaxone, amoxicillin, and ampicillin, have
been shown to elicit synergistic effects. To fight resistant bacteria, the essential oils of O. compactum
and O. elongatum, particularly those high in thymol and (E)-caryophyllene, seem promising when
combined with antibiotics. These synergistic effects could result from their ability to target the same
bacterial proteins or facilitate access to target sites, as suggested by molecular docking simulations.
Molecular dynamics simulations validated the stability of the examined protein–ligand complexes,
emphasizing the propensity of substances like thymol and (E)-caryophyllene for particular target
proteins, opening the door to potentially effective new therapeutic approaches against pathogens
resistant to multiple drugs.
Metabolites 2024, 14, 210. https://doi.org/10.3390/metabo14040210 https://www.mdpi.com/journal/metabolites