Anti-Corrosion Properties of Polyaniline/Polyurethane Composite
Coatings on Mild Steel Using Coconut-Based/PPG Blend Polyols
Marjune T. Bonilla
1,2,3,a*
, Archie G. Ruda
1,2,b
, Dave Joseph E. Estrada
4,c
,
Kurt Sterling M. Ubas
1,2,d
Aaron Andrew B. Mutia
1,2,e
,
Arnold A. Lubguban
4,f
, Rey Y. Capangpangan
5,g
, Joselito P. Labis
6,h
,
Amierson C. Tilendo
7,I
, Noel Lito B. Sayson
1,2,j
and Arnold C. Alguno
1,2,k
1
Department of Physics, MSU- Iligan Institute of Technology, Tibanga, Iligan City, Philippines
2
Premier Research of Science and Mathematics (PRISM), MSU-IIT, 9200 Iligan City, Philippines
3
University of Science and Technology of Southern Philippines
4
Bio-Products Research Laboratory, MSU-IIT, Iligan City, Lanao Del Norte, 9200, Philippines
5
Department of Physical Sciences and Mathematics, MSU-Naawan, Misamis Oriental, Philippines
6
King Abdullah Institute for Nanotechnology, King Saud University, 11451 Riyadh, Saudi Arabia
7
Mindanao State University-Main, Marawi City, Philippines
a
marjune.bonilla@g.msuiit.edu.ph and marjune.bonilla@ustp.edu.ph,
b
archie.ruda@g.msuiit.edu.ph,
c
davejoseph.estrada@g.msuiit.edu.ph,
d
kurtsterling.ubas@g.msuiit.edu.ph,
e
aaronandrew.mutia@g.msuiit.edu.ph,
f
arnold.lubguban@g.msuiit.edu.ph,
g
rycapangpangan@carsu.edu.ph,
h
jlabis@ksu.edu.sa,
i
amierson.tilendo@msumain.edu.ph,
j
noellito.sayson@g.msuiit.edu.ph, and
k
arnold.alguno@g.msuiit.edu.ph
Keywords: Polyurethane-based protective coating, coconut-based/PPG blend polyols,
Polyaniline/Polyurethane composite coatings, Potentiodynamic polarization (tafel plot), contact
angle, adhesion test, FESEM, anti-corrosion
Abstract. Polyurethane coating has been widely used as a protective coating due to its wide range of
mechanical strength, excellent abrasion resistance, toughness, low-temperature flexibility, and
chemical resistance, simplicity in production and application, and superior protection on corrosion to
mild steel. No studies have been reported utilizing coconut-based/PPG blend polyols to produce
polyurethane-based protective coatings on mild steel. Therefore, in this work, we fabricated
polyurethane-based protective coating using coconut-based/PPG blend polyols for anti-corrosion
application. Due to low adhesion strength of Polyurethane-based protective coating, the incorporation
of nano-fillers into the polymer matrix improved the adhesion strength of the coating due to its
functional benefits and its effects gave rise to increased intermolecular bonding, hydrogen bonding,
van der waals, magnetism, and surface energy. Therefore, we fabricated PANI/PU composite coatings
with varied amounts of polyaniline nanoparticles on mild steel using coconut-based/PPG blend
polyols exposed in 3.5 wt% NaCl aqueous solution for anti-corrosion application. Characterizations
like Fourier Transform Infrared Spectroscopy (FTIR), Potentiodynamic Polarization (Tafel plot),
contact angle, adhesion test, FESEM, XRD, and UV-VIS were used in this study. Tafel plot revealed
that PU-based and PANI/PU composite coatings exhibited a significant reduction in corrosion current
density (Icorr), perhaps due to the adsorption of inhibitor in the surface of the mild steel which reduced
corrosion rate of the metal by retarding the anodic process and impeding the corrosive species from
the surroundings. Among all fabricated coatings, 0.5-PANI/PU composite coating was the best,
having a less corrosion rate of 5.66x10
-5
mmpy compared to others. In addition, its surface was more
compact, smooth, rigid, and no voids present at the interface according to the result of FESEM,
suggesting better corrosion protection to mild steel. Hence, PU-based protective coating and
PANI/PU composite coatings using coconut-based/PPG blend polyols inhibited the penetration of the
corrosive species and served as an adequate barrier protection against corrosion for mild steel.
Solid State Phenomena Submitted: 2022-11-18
ISSN: 1662-9779, Vol. 351, pp 89-102 Revised: 2023-07-14
doi:10.4028/p-L7lHcU Accepted: 2023-07-15
© 2023 Trans Tech Publications Ltd, Switzerland Online: 2023-10-27
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