Int J Pharma Res Health Sci. 2019; 7 (3): 2968-73
2968
IIIIIIIII© International Journal of Pharma Research and Health Sciences. All rights reserved
DOI:10.21276/ijprhs.2019.03.03
AchorM et al CODEN (USA)-IJPRUR, e-ISSN: 2348-6465
Original Article
Synthesis of Methylcellulose from the Bark of
Crescentiacujete: Characterization and Tabletting
Properties
Achor M
1, *
, Ibrahim A T
2
, Ahmad U
2
, Nasiru A S
2
1
Faculty of Pharmaceutical Sciences, Usmanu Danfodiyo University, Sokoto.
2
Department of Pure and Applied Chemistry, Usmanu Danfodiyo University, Sokoto.
ARTICLE INFO ABSTRACT
______
1. INTRODUCTION
Cellulose is considered as an important base material for the
production of cellulose derivative such as carboxyl methyl
cellulose, methyl cellulose, hydroxy propyl methyl cellulose
1
. These derivatives are exploited by food and drug
processors and other industries to meet a specific need.
Daiyong
2
reported that wood had been the dominant
International Journal of Pharma Research and Health Sciences
Available online at www.pharmahealthsciences.net
Received: 21 Mar 2019
Accepted: 15 May2019
The methylcellulose is an important ingredient in pharmaceutical, food, cosmetic and other
industries. In this study, the methylcellulose, synthesized from the bark of Crescentia cujete,
was evaluated for its physical and tableting characteristic to assess its usefulness in
pharmaceutical tableting. The methylcellulose, synthesized from the bark of Crescentia
cujete, obtained by alkali pre-treatment, delignification followed by sodium hypochlorite
bleaching and methylation was examined for its physicochemical and tableting properties in
comparison with the well – known commercial methylcellulose and starch BP. The synthesis
yield of this methylcellulose, obtained from the bark of Crescentia cujete was approximately
83.33 % (0.8333g/g). The true density was 1.25; the flow indices showed that the
methylcellulose synthesizes from the bark of Crescentia cujete has good flow properties. The
hydration, swelling capacity were 4.40 and 466, respectively. Tablets resulting from these
methylcellulose materials were found to be without surface defects, improves the hardness
as compared to covenant methyl cellulose and starch maize, and having disintegration time
within 15 minutes. The study reveals that the methylcellulose synthesized from the bark of
Crescentia cujete compares favourably with standard and conformed to the official
requirement specified in the British Pharmacopoeia 2012 for methylcellulose.
Keywords: Characterization, Crescentia cujete, Methyl Cellulose, Tableting
Corresponding author *
Achor Mohammed
Department of Pharmaceutics and Pharmaceutical
Microbiology, Faculty of Pharmaceutical Sciences, Usmanu
Danfodiyo University, Sokoto, Nigeria
E-mail: munchors001@yahoo.com