S1
Supplementary Information
Chemoenzymatic preparation of optically active cyclic 4-hydroxy-
acylazyridines
Saúl Silva and Christopher D. Maycock
*
Instituto de Tecnologia Quı́mica e Biológica António Xavier, Universidade Nova de
Lisboa, EAN, 2780-157 Oeiras, Portugal and Departamento de Quı́mica e Bioquı́mica,
Faculdade de Ciências, Universidade de Lisboa, Campo Grande, 1749-016 Lisboa,
Portugal
* Email: maycock@itqb.unl.pt
Contents:
Table 1 – Enzymic resolution using different reaction conditions. S2
General S3
Synthesis and characterization of compounds S3-S11
References S11
Copies of the
1
H (400 MHz) and
13
C (101 MHz) APT NMR spectra for compounds 13-26, 4-(TBSO)-
cyclohept-2-en-1-one, 4-(TBSO)-2-iodocyclohept-2-en-1-one. S12-S28
Copies of the chromatograms for compounds 17-21. S29-S33
Electronic Supplementary Material (ESI) for Organic Chemistry Frontiers.
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