Proceedings of the 1
st
Annual Gas Processing Symposium
H. Alfadala, G.V. Rex Reklaitis and M.M. El-Halwagi (Editors)
© 2009 Elsevier B.V. All rights reserved. 1
Development in Mixed Refrigerant Cycles Used in
Olefin Plants
M. Mafi, M. Amidpour, and S.M. Mousavi Naeynian
Department of Mechanical Engineering, K.N.Toosi University of Technology,
No. 15, Pardis Street, Mollasadra Avenue, Vanak Suare, P.O. Box: 19395-1999,
Tehran, Iran
Abstract
Numerous mixed refrigerant cycles for separation systems of petrochemical industries
were developed in the past several decades. In this paper, two sets of low temperature
mixed refrigerant cycles were developed for a typical olefin plant utilizing a mixture of
methane, ethane, propane and nitrogen as cycle working fluid to replace the pure
ethylene refrigeration cycle which is used in conjunction with propylene refrigeration in
conventional plants. The key parameters of the two cycles were compared, and the
matching of the heating and cooling curves in heat exchangers was also analyzed. The
obtained results reveal that mixed refrigerant cycles can improve thermodynamic
performance of refrigeration systems in the case of using optimal working fluid mixture
composition, optimal high and low operating pressures and optimal arrangement of the
cycle components.
Keywords: Mixed refrigerant; Cascade refrigeration system; Olefin plant
1. Introduction
The recovery of ethylene from crude light hydrocarbon gas mixture is an economically
important but highly energy intensive process. Cryogenic separation methods are
commonly used which require large amounts of refrigeration at low temperatures and
the development of the methods to reduce net power to provide this refrigeration is
important in the petrochemical industry.
Essentially all olefin plants use an ethylene-propylene cascade refrigeration system to
provide the major portion of refrigeration required in the olefin plant. Most of the
propylene (high level) refrigeration is utilized at several pressure/temperature levels in
the initial feed precooling and fractionation sections of the plant to cool the feed from
ambient temperature to about -35°C and to condense the ethylene refrigerant at about
-30°C. Similarly, the ethylene (low level) refrigeration is utilized at several
pressure/temperature levels in the cryogenic section of the plant to cool the feed from
-35°C to about -100°C in order to condense the bulk of the ethylene in the form of
liquid feeds to a demethanizer column, and in the demethanizer column overhead
condenser at about -101°C to provide reflux to that column. Refrigeration below
-101°C, to condense the remaining ethylene from the feed, is provided primarily by
work of expansion or Joule-Thomson expansion of rejected light gases, H
2
and methane,
and/or by vaporization of methane refrigerant which has been condensed by the