Molecular Dynamics Study of Cu Thin Film Deposition on β-Ta
Peter Klaver* and Barend J. Thijsse
Delft University of Technology, Department of Materials Science,
Rotterdamseweg 137, 2628AL Delft, The Netherlands.
*t.p.c.klaver@tnw.tudelft.nl
ABSTRACT
Molecular Dynamics simulations were performed to study Cu film deposition on β-Ta. Three
different β-Ta surfaces were used, two being atomically flat, and one resulting from Ta on Ta
growth. We find that the Cu films develop a (111) texture with vertical grain boundaries between
grains having different epitaxial relations with the β-Ta substrate. The epitaxial rotation angles
were determined, as 5.2° and 10-13°, and the resulting strain reductions in the Cu films were
identified. The effects of the substrate differences on the interfacial Ta/Cu intermixing and the
epitaxy and grain boundary structure of the films are discussed.
INTRODUCTION
Copper is the metal of choice for modern IC interconnects. However, copper diffuses into
silicon and silicon oxide quite rapidly, degrading the device properties. Therefore diffusion
barriers must be used to keep copper from interacting with silicon and silicon oxide. Tantalum is
one of a number of metals and compounds under consideration for their good barrier properties.
Understanding the growth of Cu thin films on Ta substrates is therefore not only fundamentally
interesting, but also technologically relevant, since the microstructure of the Cu film affects its
adhesion to Ta and its electromigration resistance.
The purpose of this molecular dynamics simulations work is to obtain atomic-level
information on the growth of Cu films on different β-Ta substrates. β-Ta is a metastable crystal
structure frequently found in thin films. Phenomena studied include epitaxial relations, film
texture, nonequilibrium interface mixing, and defect production and evolution. This work, the
successor to our recent work on Ta on Ta deposition [1], is part of a more comprehensive
deposition study of the Cu/Ta system.
COMPUTATIONAL DETAILS
The simulations were performed using the CAMELION Molecular Dynamics code
developed in Delft [2], employing Embedded Atom Method (EAM) potentials in the Johnson-Oh
form [3,4]. We used the unlike-atom pair potential form by Johnson [5], which has only one free
parameter. This parameter was fitted to the slightly positive heat of solution (0.03 eV/atom) of a
50-50 atom% Ta-Cu random alloy. This value was determined from the Miedema model [6].
Several conditions in the simulations are copied from experiments carried out in our group,
like the slightly off-normal incidence of the Cu vapour flux (15°). The in-plane direction of each
incoming Cu atom is chosen randomly, which is intended as an “arbitrary” angle without a
specific relation to the crystal structure. The Cu atoms arrive with a thermal energy
Mat. Res. Soc. Symp. Proc. Vol. 721 © 2002 Materials Research Society
J2.3.1