INSTITUTE OF PHYSICS PUBLISHING NANOTECHNOLOGY
Nanotechnology 12 (2001) 258–264 PII: S0957-4484(01)18474-6
The effect of an electric field on the
chemical vapour deposition of (100)
diamond
Jeung Ku Kang
1
and Charles B Musgrave
1,2
1
Department of Materials Science and Engineering, Stanford University, Stanford, CA
94305-2205, USA
2
Department of Chemical Engineering, Stanford University, Stanford, CA 94305-5025, USA
Received 31 October 2000, in final form 6 March 2001
Published 24 August 2001
Online at stacks.iop.org/Nano/12/258
Abstract
The scanning tunnelling microscope (STM) has been used to modify
surfaces with atomic resolution and has consequently been proposed as a
tool for nanotechnology. Here we examine a process for deposition of (100)
diamond under a localized electric field. We use ab initio
quantum-chemistry techniques to investigate the effect of an electric field on
the chemical vapour deposition of (100) diamond. The field approximates
the field of an STM by using a point charge placed 15 Å above the surface to
create a 0.64 V Å
-1
field at the dimer. Our study explores the effect of this
electric field on CH
3
adsorption, and the dimer-opening and ring-closing
steps of the Brenner–Garrison diamond CVD mechanism. CH
3
adsorption
is exothermic by 84 kcal mol
-1
and is not affected by the electric field. The
dimer-opening and ring-closing steps are sensitive to the applied field: the
dimer-opening barrier is reduced from 9.6 to 6.0 kcal mol
-1
, while the
barrier of the ring-closing step is reduced from 13.6 to 11.0 kcal mol
-1
. Our
results indicate that the rate of CVD diamond growth can be enhanced by
the application of an electric field, in agreement with experiment.
1. Introduction
Eigler and Schweizer first used a scanning tunnelling
microscope (STM) to position individual atoms on a single-
crystal surface with atomic precision [1]. Musgrave et al [2]
later proposed a nanofabrication tool to abstract hydrogen
from a hydrogen-passivated surface using an ethynyl radical
attached to a scanning probe microscope (SPM) tip. The idea
was originally to use a radical that would form a strong enough
bond to the surface hydrogen that the abstraction barrier would
be small. The disadvantage of this tip is in that it must be
regenerated after each use. However, it is well demonstrated
that the field or current of the STM can be used to modify
a surface with atomic or nanoscale precision [3, 4]. This
approach appears to be more practical given the current state
of scanning probe technology because it does not require
the attachment or regeneration of radicals. Nanotechnology
processes that use the electric field of an STM tip to control
surface chemical reactions by either modifying activation
barriers or selecting between alternative reaction pathways will
allow us to construct a wide range of nanoscale devices. For
example, the modification of the barriers for the elementary
reaction steps of diamond growth would demonstrate that
the deposition and modification of diamond surfaces can be
controlled with an electric field to create atomically precise
components.
The growth of diamond films has been of great interest
because diamond has a wide range of electronic, mechanical
and optical properties. One reason for the wide range
of properties is the ability of carbon to adopt sp, sp
2
or
sp
3
hybridization in materials. Metal semiconductor field-
effect transistors (MESFETs) [5] fabricated on hydrogen-
terminated diamond films capable of high speed and with good
temperature stability have been demonstrated recently. This,
as well as other applications in integrated circuit technology,
has motivated efforts to grow diamond films of high quality in
the microelectronics industry. Microwave-enhanced plasma
CVD (MEPCVD) at a high ratio of CH
4
/H
2
is used for the
growth of smooth diamond films. In addition to high speed and
temperature stability, MESFETs fabricated on these films have
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