Send Orders of Reprints at reprints@benthamscience.net 370 Current Bioactive Compounds 2012, 8, 370-409 Activity and Structure Elucidation of Ceramides E. S. Elkhayat a *, G. A. Mohamed a and S. R. M. Ibrahim b a Faculty of Pharmacy, Department of Pharmacognosy, Al–Azhar University, Assiut, 71524 Egypt; b Faculty of Phar- macy, Department of Pharmacognosy, Assiut University, Assiut,71526 Egypt Abstract: Ceramide, a derivative of sphingolipid breakdown products, acts as second messenger for multiple extracellular stimuli including growth factors, chemical agents, and environmental stresses. They have been shown to be crtically in- volved in various biological processes, including differentiation, senescence, cell-cycle arrest, proliferation, and apoptosis. Ceramide molecules form distinct domains in the cell membrane, which may serve to re-organize cellular receptors and signaling molecules. Because of their promising biological activities and applications, here we focus on: biosynthesis, ex- istence, importance, and structure elucidation, as well as representative examples concerning their structure and activity. Keywords: Ceramide, sphingolipid, biological activity, identification. INTRODUCTION Ceramide is a family of lipids that consist of sphingosine linked to fatty acid via amide linkage [1]. The vast majority of fatty acids are -hydroxylated. The polyunsaturated fatty acids exist in certain testicular cells [2,3]. Ceramide plays important role in organizing membrane structure as it has the tendency to self-aggregate and segregate into membrane microdomains [4]. For years, it was assumed that ceramide was purely structural elements. This is now known to be not completely true. Ceramide attracted substantial concern be- cause of its contribution in vital biological processes such as cell cycle arrest, apoptotic cell death, cellular proliferation and inflammatory responses [5,6]. Such effects have been attributed to the second messenger signaling capabilities of this lipid. With a small hydroxy head group and two long saturated hydrophobic chains, in addition to intermolecular hydrogen bonding, ceramide packed tightly in bilayers and promotes membrane rigidity [7]. Ceramide represent precursor of major sphingolipids, such as sphingomyelin (SM), ceramides 1-phosphate (C1P), and glucosylceramides (GlcCer) [8,9]. Sphingolipids them- selves are the precursors to generate series of glycosphin- golipids and gangliosides [10,11] (Fig. 1). BIOSYNTHESIS OF CERAMIDES New approaches in cell biology and the development of in vivo models (e.g. yeast [12], Dorsophila [13], and geneti- cally modified mice [14]), afforded the identification of dif- ferent biosynthetic pathways for ceramide [15,16]. Several efforts have described the basic engagement of major phos- pholipids in biosynthesis and degradation of ceramide [4]. Ceramide could be generated by one of three main pathways; de novo synthesis, through SM hydrolysis, or through sal- vage pathway. *Address correspondence to this author at the Faculty of Pharmacy, De- partment of Pharmacognosy, Al–Azhar University, Assiut, 71524 Egypt; E-mail: khayat71@yahoo.com HO NH 3 OH Sphingosine O NH 3 OH P HO O O Sphingosine-1-phosphate O HN OH P HO O O O Ceramide-1-phosphate HO HN OH O Amide linked fatty acyl chain O HN OH P O O O O Sphingomyelin N Cerebroside O NH O OH O HO HO OH OH Fig. (1). Bioactive Sphingolipids a. Sphingomyelin Hydrolysis (Sphingomyelinase) In this pathway, ceramide was generated from hydrolysis of SM induced by the effect of sphingomyelinase (SMase) [17,18], which cleave SM to ceramide and phosphocholine. SMases are stimulated in response to TNF-[19,20], fatty acids ligand [21], or oxidative stress [22]. The SM hydroly- sis has emerged as a major pathway of stress-induced cera- mide generation. This pathway has been suggested to regu- late SM and ceramide levels [23], as well as the activation of NFB [24-26]. 1875-6646/12 $58.00+.00 © 2012 Bentham Science Publishers