VOLUME 75, NUMBER 9 PHYSICAL REVIEW LETTERS 28 AUGUST 1995 Phase Diagram and Orientational Order in a Biaxial Lattice Model: A Monte Carlo Study F. Biscarini, 1, * C. Chiccoli, 2 P. Pasini, 2 F. Semeria, 2 and C. Zannoni 1 1 Dipartimento di Chimica Fisica ed Inorganica, Università di Bologna, Viale Risorgimento 4, 40136 Bologna, Italy 2 Istituto Nazionale di Fisica Nucleare, Sezione di Bologna, Via Irnerio 46, 40126 Bologna, Italy (Received 27 March 1995) We have determined the phase diagram for a lattice system of biaxial particles interacting with a second rank anisotropic potential using Monte Carlo simulations for a number of values of the molecular biaxiality. We find increasing differences from mean field theory as the biaxiality increases. We have also calculated for the first time the full set of second rank biaxial and uniaxial order parameters and their temperature dependence, and on this basis we comment on the difficulties of measuring phase biaxiality by NMR. PACS numbers: 61.30.Gd, 61.30.Cz, 64.70.Md Liquid crystal phases formed by biaxial particles have been studied using a number of theoretical methods; e.g., without trying to be exhaustive, mean field theory (MFT) [1–4], counting methods [5], Landau–de Gennes theory [6,7], bifurcation analysis [8], density functional theory [9], etc. All the theories mentioned above predict that the system will exhibit four phases as the molecular biaxial- ity varies: a positive (N 1 ) and a negative (N 2 ) uniaxial phase, respectively, formed by prolate or oblate particles, a biaxial (N B ), and an isotropic (I ) phase. The nematic- isotropic phase transition is expected to be first order and to weaken as the biaxiality increases until it becomes con- tinuous at the point (Landau bicritical point) of maximum molecular biaxiality. At this point the system should go directly from a biaxial to an isotropic phase. The biaxial- uniaxial transition is expected to be second order. The possibility of a biaxial-nematic mesophase has been con- firmed by some computer simulations of a lattice system of biaxial particles [10,11], and of a fluid system of biax- ial spherocylinders [12]. On the experimental side, there is an increasing number of biaxial lyotropic [13] and poly- meric [14] phases while the observation of thermotropic, claimed by a number of authors [15], typically on the ba- sis of optical observations, is still questioned [16]. Given this extensive activity, it is surprising that a de- tailed computer experimental study of the phase diagram and, even more, of the full set of order parameters and their detailed temperature dependence within the biaxial and uniaxial phases are not available as yet. This informa- tion is crucial for the study of static but also, indirectly, of dynamic properties [17] and in general to validate molecu- lar theories. In this Letter we make an attack on this prob- lem and we propose a general prescription for calculating order parameters from simulations in systems with sym- metry lower than uniaxial. We base our calculations on the simplest second rank attractive pair potential [3,10], Uv ij 2e ij P 2 cos b ij 1 2lR 2 02 v ij 1 R 2 20 v ij  1 4l 2 R 2 22 v ij  , (1) with the biaxial molecules, or “spins,” fixed at the sites of a three-dimensional cubic lattice. The coupling parameter e ij is taken to be a positive constant e when particles i and j are nearest neighbors and zero otherwise. v ij is the relative orientation of the molecular pair, given by three Euler angles a, b, and g [18]. P 2 is a second Legendre polynomial and R L mn are combinations of Wigner functions D L mn [18] symmetry-adapted for the D 2h group of the two particles. Their explicit expressions, for the even terms, are R L mn 1 2 ReD L mn 1 D L m2n . (2) The biaxiality parameter l accounts for the deviation from cylindrical molecular symmetry: when l is zero, the po- tential Eq. (1) reduces to the well-known Lebwohl-Lasher P 2 potential [19], while for l different from zero the par- ticles tend to align not only their major axis, but also their faces. The value l 1 p 6 marks the boundary between a system of prolate l, 1 p 6 and oblate molecules l. 1 p 6 and is analogous to the self-dual case de- scribed by Straley [2]. Thermodynamic results for a pro- late particle at biaxiality l and T kT e can be mapped onto l 0 , T 0 3 2l p 6  p 6 1 6l, 24T 6l1 p 6 2 for the dual oblate particle. We have performed Monte Carlo (MC) simulations [19] for 16 values of the biaxiality parameter l, both on an 8 3 8 3 8 and a 10 3 10 3 10 lattice. For each l value, about 40 temperatures have been investigated. For l 0.3 additional larger size simulations (40 3 40 3 40) have been performed at selected temperatures near the biaxial-nematic and nematic-isotropic transitions to rule out system size artifacts. The Metropolis MC method with periodic boundary conditions and controlled angu- lar displacement [19,20] has been employed for lattice updates. We have typically used 30 000 lattice sweeps (cycles) for equilibration and 20 000 for production. The 40 3 40 3 40 system has required 40 and 30 kcycles. In Fig. 1 we show the heat capacity C V obtained by dif- ferentiating the energy against temperature as described in [20] and plotted against temperature for l 0.2, 0.3, and 0.408 25. Starting with the lower values of l, we see that C V exhibits a small peak at low temperature 0031-90079575(9) 1803(4)$06.00 © 1995 The American Physical Society 1803