Academic Research International Vol. 5(4) July 2014
Copyright © 2014 SAVAP International ISSN: 2223-9944, e ISSN: 2223-9553
www.savap.org.pk 60 www.journals.savap.org.pk
Heterogeneous Catalytic Modified Process in the Production of Biodiesel
from Sunflower Oil, Waste Cooking Oil and Olive Oil by
Transesterification Method
KambizTahvildari
1
, Hamid Reza Chitsaz
2
, Paria Mozaffarinia
3
Islamic Azad University, Tehran-North Branch, IRAN.
K_tahvildari@iau-tnb.ac.ir
ABSTRACT
Using transesterifiction of sunflower oil, olive oil and waste cooking oil with
methanol and heterogeneous catalyst made by clinoptilolite, biodiesel was obtained.
With molar ratio of alcohol to oil 1:7 and mentioned catalyst (3 wt%), yield of
biodiesel from sunflower oil, cooking waste oil and olive oil were: 97%, 95% & 92%
respectively. SEM images showed the average particle sizeof 342.44 nm. FTIR
spectrum showedno impurity in produced biodiesel. The products were compared to
the consuming Petro-dieselin Tehran according ASTM standard cloud point, pour
point, freezing point, cetane number, iodine value, saponification number, heating
value, acid value, viscosity, density andflash point.
Keywords: Biodiesel, transesterifiction, clinoptilolite, waste cooking oil, sunflower
oil, olive oil
INTRODUCTION
Biodiesel has attracted much attention because it is biodegradable, renewable, and is non-
toxic (importantly when fuels leak into the environment). The fuel is free of sulfur and
aromatics, while petro-diesel fuel may contain 500 ppm sulfur dioxide and 20-40wt%
aromatics [1-5]. Recent studies showed that applying biodiesel may reduce various cancers
and toxic aerosols by 95% and 90% respectively, which resulted in improved environmental
condition [6 ,7].
More than 350 different oilseeds already have been found throughout the world that have the
potential to produce biodiesel[8]. In general, the main sources are classified into four
categories as below [9,10]:
1- Animal fats: chicken fat and lard
2- Edible vegetable oil: sunflower, soybean, olive and coconut
3- Inedible vegetable oil: Jatrophacurcas, Calophylluminophyllum, Moringaoleifera
and Croton megalocarpus
4- Waste cooking oil and recycled oil
Biodiesel can be used in any mixture with petro-diesel fuel, as it has very similar
characteristics (cetane number, viscosity, heating value, etc)[11,12]and also in any diesel
engine without modification [13,14]. Biodiesel density affects engine fuel injection system.
Lower fuel density and viscosity will lead to more improved atomization and mixing
characteristics. Higher density cause increased particulateemission and NOx. Low density
indicates decreased saturated hydrocarbon chain. The viscosity of the fuel depends on its
structure and decreases by increasing double bonds. Biodiesel freezing point will increase by